1,4-Dimethyl-3-oxa-6,7-diaza-tricyclo[3.3.0.0^2,4]octane-6,7-dicarboxylic acid 7-benzyl ester 6-ethyl ester

Base Information

• Chemical Name: 1,4-Dimethyl-3-oxa-6,7-diaza-tricyclo[3.3.0.0^2,4]octane-6,7-dicarboxylic acid 7-benzyl ester 6-ethyl ester
• CAS No.: 121682-08-4
• Molecular Formula: C₁₈H₂₂N₂O₅
• Molecular Weight: 346.383

Synonyms:1,4-Dimethyl-3-oxa-6,7-diaza-tricyclo[3.3.0.0^2,4]octane-6,7-dicarboxylic acid 7-benzyl ester 6-ethyl ester

Chemical Property of 1,4-Dimethyl-3-oxa-6,7-diaza-tricyclo[3.3.0.0^2,4]octane-6,7-dicarboxylic acid 7-benzyl ester 6-ethyl ester

Chemical Property:

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Technology Process of 1,4-Dimethyl-3-oxa-6,7-diaza-tricyclo[3.3.0.0^2,4]octane-6,7-dicarboxylic acid 7-benzyl ester 6-ethyl ester

There total 5 articles about 1,4-Dimethyl-3-oxa-6,7-diaza-tricyclo[3.3.0.0^2,4]octane-6,7-dicarboxylic acid 7-benzyl ester 6-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

5,7-Dimethyl-2,3-diaza-bicyclo[3.2.0]hept-6-ene-2,3-dicarboxylic acid 3-benzyl ester 2-ethyl ester (121682-07-3) → 1,4-Dimethyl-3-oxa-6,7-diaza-tricyclo[3.3.0.02,4]octane-6,7-dicarboxylic acid 7-benzyl ester 6-ethyl ester (121682-08-4)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 10h; Ambient temperature;

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → 1,4-Dimethyl-3-oxa-6,7-diaza-tricyclo[3.3.0.02,4]octane-6,7-dicarboxylic acid 7-benzyl ester 6-ethyl ester (121682-08-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / potassium carbonate / ethanol / 8 h / Ambient temperature

2: 95 percent / m-chloroperbenzoic acid (m-CPBA) / CH₂Cl₂ / 10 h / Ambient temperature

With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane;

Reference yield:

4,6-Dimethyl-2,3-dihydro-[1,2]diazepine-1-carboxylic acid ethyl ester (121682-05-1) → 1,4-Dimethyl-3-oxa-6,7-diaza-tricyclo[3.3.0.02,4]octane-6,7-dicarboxylic acid 7-benzyl ester 6-ethyl ester (121682-08-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 84 percent / benzene / 15 h / Irradiation

2: 95 percent / potassium carbonate / ethanol / 8 h / Ambient temperature

3: 95 percent / m-chloroperbenzoic acid (m-CPBA) / CH₂Cl₂ / 10 h / Ambient temperature

With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane; benzene;

upstream raw materials:

5,7-Dimethyl-2,3-diaza-bicyclo[3.2.0]hept-6-ene-2,3-dicarboxylic acid 3-benzyl ester 2-ethyl ester

benzyl chloroformate

4,6-Dimethyl-2,3-dihydro-[1,2]diazepine-1-carboxylic acid ethyl ester

5,7-Dimethyl-2,3-diaza-bicyclo[3.2.0]hept-6-ene-2-carboxylic acid ethyl ester

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