benzyl N-[(2S)-1-{[(2S)-2-{[(benzyloxy)carbonyl]amino}-4-[(2,2-dimethylpropoxy)sulfonyl]butyl]disulfanyl}-4-[(2,2-dimethylpropoxy)sulfonyl]butan-2-yl]carbamate

Base Information

Chemical Name:benzyl N-[(2S)-1-{[(2S)-2-{[(benzyloxy)carbonyl]amino}-4-[(2,2-dimethylpropoxy)sulfonyl]butyl]disulfanyl}-4-[(2,2-dimethylpropoxy)sulfonyl]butan-2-yl]carbamate
CAS No.:1370348-27-8
Molecular Formula:C₃₄H₅₂N₂O₁₀S₄
Molecular Weight:777.058
Hs Code.:

benzyl N-[(2S)-1-{[(2S)-2-{[(benzyloxy)carbonyl]amino}-4-[(2,2-dimethylpropoxy)sulfonyl]butyl]disulfanyl}-4-[(2,2-dimethylpropoxy)sulfonyl]butan-2-yl]carbamate

Synonyms:benzyl N-[(2S)-1-{[(2S)-2-{[(benzyloxy)carbonyl]amino}-4-[(2,2-dimethylpropoxy)sulfonyl]butyl]disulfanyl}-4-[(2,2-dimethylpropoxy)sulfonyl]butan-2-yl]carbamate

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Chemical Property of benzyl N-[(2S)-1-{[(2S)-2-{[(benzyloxy)carbonyl]amino}-4-[(2,2-dimethylpropoxy)sulfonyl]butyl]disulfanyl}-4-[(2,2-dimethylpropoxy)sulfonyl]butan-2-yl]carbamate

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Technology Process of benzyl N-[(2S)-1-{[(2S)-2-{[(benzyloxy)carbonyl]amino}-4-[(2,2-dimethylpropoxy)sulfonyl]butyl]disulfanyl}-4-[(2,2-dimethylpropoxy)sulfonyl]butan-2-yl]carbamate

There total 9 articles about benzyl N-[(2S)-1-{[(2S)-2-{[(benzyloxy)carbonyl]amino}-4-[(2,2-dimethylpropoxy)sulfonyl]butyl]disulfanyl}-4-[(2,2-dimethylpropoxy)sulfonyl]butan-2-yl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₇NO₅S₂

: 1370348-27-8
benzyl N-[(2S)-1-{[(2S)-2-{[(benzyloxy)carbonyl]amino}-4-[(2,2-dimethylpropoxy)sulfonyl]butyl]disulfanyl}-4-[(2,2-dimethylpropoxy)sulfonyl]butan-2-yl]carbamate

Guidance literature:: With sodium disulfite; iodine; In ethanol; water; at 20 ℃;

Reference yield:

: 66076-71-9
N,N'-di(CBz)-L-homocystine

: 1370348-27-8
benzyl N-[(2S)-1-{[(2S)-2-{[(benzyloxy)carbonyl]amino}-4-[(2,2-dimethylpropoxy)sulfonyl]butyl]disulfanyl}-4-[(2,2-dimethylpropoxy)sulfonyl]butan-2-yl]carbamate

Guidance literature:: Multi-step reaction with 8 steps

1: thionyl chloride / 1 h / 50 °C

2: sulfuryl dichloride / ethanol / 5 - 10 °C

3: triethylamine / toluene / 0 - 20 °C

4: lithium borohydride / tetrahydrofuran / 3 h / 20 °C

5: triethylamine / toluene; tert-butyl methyl ether / 10 - 20 °C

6: acetone / 2 h / 20 °C

7: sodium hydroxide; water / ethanol / 0 - 10 °C

8: sodium disulfite; iodine / ethanol; water / 20 °C

With sodium disulfite; lithium borohydride; thionyl chloride; sulfuryl dichloride; water; iodine; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; tert-butyl methyl ether; water; acetone; toluene;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1370348-27-8
benzyl N-[(2S)-1-{[(2S)-2-{[(benzyloxy)carbonyl]amino}-4-[(2,2-dimethylpropoxy)sulfonyl]butyl]disulfanyl}-4-[(2,2-dimethylpropoxy)sulfonyl]butan-2-yl]carbamate

Guidance literature:: Multi-step reaction with 9 steps

1: sodium hydroxide / water; tetrahydrofuran / 5 - 20 °C

2: thionyl chloride / 1 h / 50 °C

3: sulfuryl dichloride / ethanol / 5 - 10 °C

4: triethylamine / toluene / 0 - 20 °C

5: lithium borohydride / tetrahydrofuran / 3 h / 20 °C

6: triethylamine / toluene; tert-butyl methyl ether / 10 - 20 °C

7: acetone / 2 h / 20 °C

8: sodium hydroxide; water / ethanol / 0 - 10 °C

9: sodium disulfite; iodine / ethanol; water / 20 °C

With sodium disulfite; lithium borohydride; thionyl chloride; sulfuryl dichloride; water; iodine; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; tert-butyl methyl ether; water; acetone; toluene;