Benzyl-carbamic acid (1S,2S,5S)-1-methyl-6-oxa-bicyclo[3.1.0]hex-2-yl ester

Base Information

Chemical Name:Benzyl-carbamic acid (1S,2S,5S)-1-methyl-6-oxa-bicyclo[3.1.0]hex-2-yl ester
CAS No.:126059-86-7
Molecular Formula:C₁₄H₁₇NO₃
Molecular Weight:247.294
Hs Code.:

Synonyms:Benzyl-carbamic acid (1S,2S,5S)-1-methyl-6-oxa-bicyclo[3.1.0]hex-2-yl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl-carbamic acid (1S,2S,5S)-1-methyl-6-oxa-bicyclo[3.1.0]hex-2-yl ester

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Technology Process of Benzyl-carbamic acid (1S,2S,5S)-1-methyl-6-oxa-bicyclo[3.1.0]hex-2-yl ester

There total 3 articles about Benzyl-carbamic acid (1S,2S,5S)-1-methyl-6-oxa-bicyclo[3.1.0]hex-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119449-79-5
Benzyl-carbamic acid 2-methyl-cyclopent-2-enyl ester

: 126059-86-7
Benzyl-carbamic acid (1S,2S,5S)-1-methyl-6-oxa-bicyclo[3.1.0]hex-2-yl ester

: 126059-85-6
(1R^*,2S^*,3S^*)-1-<(N-Benzylcarbamoyl)oxy>-2-methyl-2,3-epoxycyclopentane

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃;
DOI:10.1021/jo00297a047

Reference yield:

: 108297-40-1
(+/-)-2-methylcyclopent-2-enol

: 126059-86-7
Benzyl-carbamic acid (1S,2S,5S)-1-methyl-6-oxa-bicyclo[3.1.0]hex-2-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 72 h / Ambient temperature

2: MCPBA (m-chloroperoxybenzoic acid) / 0 °C / CH₂Cl₂ or CHCl₃

With 3-chloro-benzenecarboperoxoic acid;
DOI:10.1016/S0040-4039(00)87911-3

Reference yield:

: 3173-56-6
benzyl isothiocyanate

: 126059-86-7
Benzyl-carbamic acid (1S,2S,5S)-1-methyl-6-oxa-bicyclo[3.1.0]hex-2-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 72 h / Ambient temperature

2: MCPBA (m-chloroperoxybenzoic acid) / 0 °C / CH₂Cl₂ or CHCl₃

With 3-chloro-benzenecarboperoxoic acid;
DOI:10.1016/S0040-4039(00)87911-3