N-(6-[(1,1-dimethylethyl)dimethylsilyloxy]hexyloxy)(4,4'-dimethoxytriphenylmethyl)amine

Base Information

Chemical Name:N-(6-[(1,1-dimethylethyl)dimethylsilyloxy]hexyloxy)(4,4'-dimethoxytriphenylmethyl)amine
CAS No.:300575-18-2
Molecular Formula:C₃₃H₄₇NO₄Si
Molecular Weight:549.826
Hs Code.:

Synonyms:N-(6-[(1,1-dimethylethyl)dimethylsilyloxy]hexyloxy)(4,4'-dimethoxytriphenylmethyl)amine

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Chemical Property of N-(6-[(1,1-dimethylethyl)dimethylsilyloxy]hexyloxy)(4,4'-dimethoxytriphenylmethyl)amine

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Technology Process of N-(6-[(1,1-dimethylethyl)dimethylsilyloxy]hexyloxy)(4,4'-dimethoxytriphenylmethyl)amine

There total 4 articles about N-(6-[(1,1-dimethylethyl)dimethylsilyloxy]hexyloxy)(4,4'-dimethoxytriphenylmethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 300575-16-0
(6-[(1,1-dimethylethyl)dimethylsilyloxy]hexyloxy)amine

: 300575-18-2
N-(6-[(1,1-dimethylethyl)dimethylsilyloxy]hexyloxy)(4,4'-dimethoxytriphenylmethyl)amine

Guidance literature:: With triethylamine; In dichloromethane; Heating;
DOI:10.1071/ch00018

Reference yield:

: 4286-55-9
1-bromo-6-hexanol

: 300575-18-2
N-(6-[(1,1-dimethylethyl)dimethylsilyloxy]hexyloxy)(4,4'-dimethoxytriphenylmethyl)amine

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / K₂CO₃ / dimethylsulfoxide / 0.5 h / 70 °C

2: 82 percent / diisopropylethylamine / CH₂Cl₂ / 6 h / 20 °C

3: 80 percent / hydrazine monohydrate / methanol / 2 h / 60 °C

4: 94 percent / Et₃N / CH₂Cl₂ / Heating

With potassium carbonate; hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; dimethyl sulfoxide; 1: Alkylation / 2: silylation / 3: hydrazinolysis / 4: Condensation;
DOI:10.1071/ch00018

Reference yield:

: 209973-05-7
N-(6-hydroxyhexyloxy)phthalimide

: 300575-18-2
N-(6-[(1,1-dimethylethyl)dimethylsilyloxy]hexyloxy)(4,4'-dimethoxytriphenylmethyl)amine

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / diisopropylethylamine / CH₂Cl₂ / 6 h / 20 °C

2: 80 percent / hydrazine monohydrate / methanol / 2 h / 60 °C

3: 94 percent / Et₃N / CH₂Cl₂ / Heating

With hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; 1: silylation / 2: hydrazinolysis / 3: Condensation;
DOI:10.1071/ch00018