(2R,3S)-(-)-2-methoxymethoxy-3-methyl-7-(tert-butyldiphenylsilyloxy)heptanal

Base Information

Chemical Name:(2R,3S)-(-)-2-methoxymethoxy-3-methyl-7-(tert-butyldiphenylsilyloxy)heptanal
CAS No.:1245634-53-0
Molecular Formula:C₂₆H₃₈O₄Si
Molecular Weight:442.671
Hs Code.:

Synonyms:(2R,3S)-(-)-2-methoxymethoxy-3-methyl-7-(tert-butyldiphenylsilyloxy)heptanal

Suppliers and Price of (2R,3S)-(-)-2-methoxymethoxy-3-methyl-7-(tert-butyldiphenylsilyloxy)heptanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S)-(-)-2-methoxymethoxy-3-methyl-7-(tert-butyldiphenylsilyloxy)heptanal

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Technology Process of (2R,3S)-(-)-2-methoxymethoxy-3-methyl-7-(tert-butyldiphenylsilyloxy)heptanal

There total 1 articles about (2R,3S)-(-)-2-methoxymethoxy-3-methyl-7-(tert-butyldiphenylsilyloxy)heptanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1245634-76-7
C₂₆H₄₀O₄Si

: 1245634-53-0
(2R,3S)-(-)-2-methoxymethoxy-3-methyl-7-(tert-butyldiphenylsilyloxy)heptanal

Guidance literature:: C₂₆H₄₀O₄Si; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.166667h;

With triethylamine; In dichloromethane; for 0.5h;
DOI:10.1021/ol101776e

Reference yield:

: methyl (Z)-2-(bromomethyl)-5-methyl-2-hexenoate

: 1245634-53-0
(2R,3S)-(-)-2-methoxymethoxy-3-methyl-7-(tert-butyldiphenylsilyloxy)heptanal

: 1245634-54-1
C₃₄H₅₀O₅Si

: 1245634-55-2
C₃₄H₅₀O₅Si

Guidance literature:: methyl (Z)-2-(bromomethyl)-5-methyl-2-hexenoate; (2R,3S)-(-)-2-methoxymethoxy-3-methyl-7-(tert-butyldiphenylsilyloxy)heptanal; With chromium dichloride; In tetrahydrofuran; at 20 ℃; for 4h; Inert atmosphere;

With toluene-4-sulfonic acid; In toluene; at 20 ℃; for 26h; Inert atmosphere;
DOI:10.1021/ol101776e