2-butyl-4-chloro-1-<<2'-(1H-tetrazol-5-yl)biphenyl-4-yl>methyl>imidazole-5-carboxaldehyde benzenesulfonylhydrazone

Base Information

Chemical Name:2-butyl-4-chloro-1-<<2'-(1H-tetrazol-5-yl)biphenyl-4-yl>methyl>imidazole-5-carboxaldehyde benzenesulfonylhydrazone
CAS No.:124750-13-6
Molecular Formula:C₂₈H₂₇ClN₈O₂S
Molecular Weight:575.094
Hs Code.:

Synonyms:2-butyl-4-chloro-1-<<2'-(1H-tetrazol-5-yl)biphenyl-4-yl>methyl>imidazole-5-carboxaldehyde benzenesulfonylhydrazone

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Chemical Property of 2-butyl-4-chloro-1-<<2'-(1H-tetrazol-5-yl)biphenyl-4-yl>methyl>imidazole-5-carboxaldehyde benzenesulfonylhydrazone

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Technology Process of 2-butyl-4-chloro-1-<<2'-(1H-tetrazol-5-yl)biphenyl-4-yl>methyl>imidazole-5-carboxaldehyde benzenesulfonylhydrazone

There total 12 articles about 2-butyl-4-chloro-1-<<2'-(1H-tetrazol-5-yl)biphenyl-4-yl>methyl>imidazole-5-carboxaldehyde benzenesulfonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 114798-36-6
2-n-Butyl-4-chloro-1-[(2'-(1H-tetrazol-5-yl)biphenyl-4-yl)methyl]-imidazole-5-carboxaldehyde

: 80-17-1
benzenesufonyl hydrazide

: 124750-13-6
2-butyl-4-chloro-1-<<2'-(1H-tetrazol-5-yl)biphenyl-4-yl>methyl>imidazole-5-carboxaldehyde benzenesulfonylhydrazone

Guidance literature:: With sodium hydroxide; at 25 ℃; for 18h;
DOI:10.1021/jm00112a031

Reference yield:

: 57598-33-1
2-(2-methoxyphenyl)-4,4-dimethyl-2-oxazoline

: 124750-13-6
2-butyl-4-chloro-1-<<2'-(1H-tetrazol-5-yl)biphenyl-4-yl>methyl>imidazole-5-carboxaldehyde benzenesulfonylhydrazone

Guidance literature:: Multi-step reaction with 7 steps

1: tetrahydrofuran / 2 h / 20 °C

2: 96 percent / pyridine, phosphorus oxychloride / 3 h / 100 °C

3: 1.) tributyltin chloride, sodium azide, 2.) 10 N aq. sodium hydroxide / 1.) toluene, reflux, 70 h, 20 deg C, 3 h

4: 92 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl₄ / 3 h / Heating

5: 49 percent / potassium carbonate / dimethylformamide / 24 h / 25 °C

6: 10percent HCl / tetrahydrofuran / 4 h / 25 °C

7: 62 percent / 1.000 N aq. NaOH / 18 h / 25 °C

With pyridine; hydrogenchloride; sodium hydroxide; N-Bromosuccinimide; sodium azide; tributyltin chloride; potassium carbonate; trichlorophosphate; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00112a031

Reference yield:

: 114772-53-1
2-Cyano-4'-methylbiphenyl

: 124750-13-6
2-butyl-4-chloro-1-<<2'-(1H-tetrazol-5-yl)biphenyl-4-yl>methyl>imidazole-5-carboxaldehyde benzenesulfonylhydrazone

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) tributyltin chloride, sodium azide, 2.) 10 N aq. sodium hydroxide / 1.) toluene, reflux, 70 h, 20 deg C, 3 h

2: 92 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl₄ / 3 h / Heating

3: 49 percent / potassium carbonate / dimethylformamide / 24 h / 25 °C

4: 10percent HCl / tetrahydrofuran / 4 h / 25 °C

5: 62 percent / 1.000 N aq. NaOH / 18 h / 25 °C

With hydrogenchloride; sodium hydroxide; N-Bromosuccinimide; sodium azide; tributyltin chloride; potassium carbonate; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00112a031