Technology Process of C37H42O6
There total 8 articles about C37H42O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C29H34O5;
With
sodium hydride;
In
tetrahydrofuran; mineral oil;
at 21 ℃;
for 0.5h;
p-methoxybenzyl chloride;
In
tetrahydrofuran; mineral oil;
at 21 ℃;
for 12h;
DOI:10.1016/j.tet.2011.10.024
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: copper(I) bromide dimethylsulfide complex / tetrahydrofuran; diethyl ether
1.2: 12 h / -30 - 0 °C
2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 21 °C
2.2: 12 h / 21 °C
With
copper(I) bromide dimethylsulfide complex; sodium hydride;
In
tetrahydrofuran; diethyl ether; mineral oil;
DOI:10.1016/j.tet.2011.10.024
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: diisobutylaluminium hydride / hexane; dichloromethane / 21 °C
2.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / decane; dichloromethane / Molecular sieve
3.1: copper(I) bromide dimethylsulfide complex / tetrahydrofuran; diethyl ether
3.2: 12 h / -30 - 0 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 21 °C
4.2: 12 h / 21 °C
With
titanium(IV) isopropylate; tert.-butylhydroperoxide; copper(I) bromide dimethylsulfide complex; L-(+)-diisopropyl tartrate; sodium hydride; diisobutylaluminium hydride;
In
tetrahydrofuran; diethyl ether; decane; hexane; dichloromethane; mineral oil;
2.1: Sharpless epoxidation;
DOI:10.1016/j.tet.2011.10.024
