(1-(4-((5-(1,3-dioxolan-2-yl)pentyl)oxy)benzyl)piperidin-4-yl)methyl 2-hydroxy-2,2-diphenylacetate

Base Information

Chemical Name:(1-(4-((5-(1,3-dioxolan-2-yl)pentyl)oxy)benzyl)piperidin-4-yl)methyl 2-hydroxy-2,2-diphenylacetate
CAS No.:1415971-32-2
Molecular Formula:C₃₅H₄₃NO₆
Molecular Weight:573.73
Hs Code.:

Synonyms:(1-(4-((5-(1,3-dioxolan-2-yl)pentyl)oxy)benzyl)piperidin-4-yl)methyl 2-hydroxy-2,2-diphenylacetate

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Chemical Property of (1-(4-((5-(1,3-dioxolan-2-yl)pentyl)oxy)benzyl)piperidin-4-yl)methyl 2-hydroxy-2,2-diphenylacetate

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Technology Process of (1-(4-((5-(1,3-dioxolan-2-yl)pentyl)oxy)benzyl)piperidin-4-yl)methyl 2-hydroxy-2,2-diphenylacetate

There total 2 articles about (1-(4-((5-(1,3-dioxolan-2-yl)pentyl)oxy)benzyl)piperidin-4-yl)methyl 2-hydroxy-2,2-diphenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 1415971-30-0
4-((5-(1,3-dioxolan-2-yl)pentyl)oxy)benzaldehyde

: 1415971-38-8
(piperidin-4-yl)methyl 2-hydroxy-2,2-diphenylacetate

: 1415971-32-2
(1-(4-((5-(1,3-dioxolan-2-yl)pentyl)oxy)benzyl)piperidin-4-yl)methyl 2-hydroxy-2,2-diphenylacetate

Guidance literature:: 4-((5-(1,3-dioxolan-2-yl)pentyl)oxy)benzaldehyde; (piperidin-4-yl)methyl 2-hydroxy-2,2-diphenylacetate; With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; for 18h;

With water; sodium hydrogencarbonate; In dichloromethane; ethyl acetate;

Reference yield:

: 56741-68-5
2-(5-bromopentyl)-1,3-dioxolane

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1415971-32-2
(1-(4-((5-(1,3-dioxolan-2-yl)pentyl)oxy)benzyl)piperidin-4-yl)methyl 2-hydroxy-2,2-diphenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 50 °C

2: sodium tris(acetoxy)borohydride / dichloromethane / 18 h / 20 °C

With sodium tris(acetoxy)borohydride; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;