(S)-2-[((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionyl)-methyl-amino]-3-phenyl-propionic acid benzyl ester

Base Information

Chemical Name:(S)-2-[((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionyl)-methyl-amino]-3-phenyl-propionic acid benzyl ester
CAS No.:174602-83-6
Molecular Formula:C₃₁H₃₆N₂O₅
Molecular Weight:516.637
Hs Code.:

Synonyms:(S)-2-[((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionyl)-methyl-amino]-3-phenyl-propionic acid benzyl ester

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Chemical Property of (S)-2-[((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionyl)-methyl-amino]-3-phenyl-propionic acid benzyl ester

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Technology Process of (S)-2-[((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionyl)-methyl-amino]-3-phenyl-propionic acid benzyl ester

There total 2 articles about (S)-2-[((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionyl)-methyl-amino]-3-phenyl-propionic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 174602-83-6
(S)-2-[((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionyl)-methyl-amino]-3-phenyl-propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine (NMM)

With 4-methyl-morpholine;
DOI:10.1016/0040-4039(96)01199-9

Reference yield:

: 40298-25-7
(S)-2-Methylamino-3-phenyl-propionic acid benzyl ester; compound with toluene-4-sulfonic acid

: C₁₉H₂₇NO₅

: 174602-83-6
(S)-2-[((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionyl)-methyl-amino]-3-phenyl-propionic acid benzyl ester

Guidance literature:: Yield given;
DOI:10.1016/0040-4039(96)01199-9

Reference yield:

: 174602-83-6
(S)-2-[((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionyl)-methyl-amino]-3-phenyl-propionic acid benzyl ester

: 127785-64-2
aureobasidin A

Guidance literature:: Multi-step reaction with 12 steps

1: H₂ / 10percent Pd/C

2: N-methylmorpholine (NMM)

4: H₂ / 10percent Pd/C

5: N-methylmorpholine (NMM)

7: H₂ / 10percent Pd/C

8: N-methylmorpholine (NMM)

10: H₂ / 10percent Pd/C

11: 1.) 50percent TFA; 2.) 1N HCl / 1.) CH₂Cl₂

12: benzotriazol-1-yloxy-tris(dimethylamino)phosphonium hexafluorophosphate (BOP), DMAP / CH₂Cl₂

With 4-methyl-morpholine; hydrogenchloride; dmap; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane;
DOI:10.1016/0040-4039(96)01199-9