6-amino-2,5:3,4-dianhydro-1,6-dideoxy-D-galacticol p-toluenesulfonate

Base Information

Chemical Name:6-amino-2,5:3,4-dianhydro-1,6-dideoxy-D-galacticol p-toluenesulfonate
CAS No.:100778-47-0
Molecular Formula:C₆H₁₁NO₂*C₇H₈O₃S
Molecular Weight:301.364
Hs Code.:

Synonyms:6-amino-2,5:3,4-dianhydro-1,6-dideoxy-D-galacticol p-toluenesulfonate

Suppliers and Price of 6-amino-2,5:3,4-dianhydro-1,6-dideoxy-D-galacticol p-toluenesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 6-amino-2,5:3,4-dianhydro-1,6-dideoxy-D-galacticol p-toluenesulfonate

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

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Technology Process of 6-amino-2,5:3,4-dianhydro-1,6-dideoxy-D-galacticol p-toluenesulfonate

There total 4 articles about 6-amino-2,5:3,4-dianhydro-1,6-dideoxy-D-galacticol p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 2,5-anhydro-6-azido-1,6-dideoxy-4-O-p-tolylsulfonyl-D-glucitol

: 100778-47-0
6-amino-2,5:3,4-dianhydro-1,6-dideoxy-D-galacticol p-toluenesulfonate

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; for 24h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90734-1

Reference yield:

: 100778-34-5
3-O-acetyl-2,5-anhydro-6-bromo-1,6-dideoxy-4-O-p-tolylsulfonyl-D-glucitol

: 100778-47-0
6-amino-2,5:3,4-dianhydro-1,6-dideoxy-D-galacticol p-toluenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / sodium azide / dimethylformamide; H₂O / 1 h / 100 °C

2: 91.7 percent / 1.5 M methanolic hydrogen chloride / 45 h / Heating

3: 40 percent / H₂, 1 M methanolic hydrogen chloride / 10 percent Pd/C / ethanol / 24 h / Ambient temperature

With hydrogenchloride; sodium azide; hydrogen; palladium on activated charcoal; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90734-1

Reference yield:

: 3-O-acetyl-2,5-anhydro-6-azido-1,6-dideoxy-4-O-p-tolylsulfonyl-D-glucitol

: 100778-47-0
6-amino-2,5:3,4-dianhydro-1,6-dideoxy-D-galacticol p-toluenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 91.7 percent / 1.5 M methanolic hydrogen chloride / 45 h / Heating

2: 40 percent / H₂, 1 M methanolic hydrogen chloride / 10 percent Pd/C / ethanol / 24 h / Ambient temperature

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0008-6215(00)90734-1