C₃₃H₂₆N₈O₇

Base Information

Chemical Name:C₃₃H₂₆N₈O₇
CAS No.:1309750-79-5
Molecular Formula:C₃₃H₂₆N₈O₇
Molecular Weight:646.619
Hs Code.:

C<sub>33</sub>H<sub>26</sub>N<sub>8</sub>O<sub>7</sub>

Synonyms:C₃₃H₂₆N₈O₇

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Chemical Property of C₃₃H₂₆N₈O₇

Chemical Property:

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Technology Process of C₃₃H₂₆N₈O₇

There total 15 articles about C₃₃H₂₆N₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94111-79-2
methyl 6-(chlorocarbonyl)picolinate

: 1309750-79-5
C₃₃H₂₆N₈O₇

Guidance literature:: Multi-step reaction with 7 steps

1: sodium azide / tetrahydrofuran; water; N,N-dimethyl-formamide / 0.5 h / Cooling

2: toluene / 30 h / 120 °C

3: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 50 °C

4: triethylamine / dichloromethane / 1 h / 20 °C

5: sodium hydroxide / water / 20 °C

6: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 2 h

7: triethylamine / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

With sodium azide; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c1cc11532d

Reference yield:

: C₈H₆N₄O₃

: 1309750-79-5
C₃₃H₂₆N₈O₇

Guidance literature:: Multi-step reaction with 6 steps

1: toluene / 30 h / 120 °C

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 50 °C

3: triethylamine / dichloromethane / 1 h / 20 °C

4: sodium hydroxide / water / 20 °C

5: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 2 h

6: triethylamine / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

With oxalyl dichloride; palladium 10% on activated carbon; hydrogen; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c1cc11532d

Reference yield:

: 5453-67-8
2,6-bis(methoxycarbonyl)pyridine

: 1309750-79-5
C₃₃H₂₆N₈O₇

Guidance literature:: Multi-step reaction with 9 steps

1: sodium hydroxide / water / 12 h / 20 °C

2: 4-methyl-morpholine; chloroformic acid ethyl ester / tetrahydrofuran; N,N-dimethyl-formamide / 0.25 h / -10 - -5 °C

3: sodium azide / tetrahydrofuran; water; N,N-dimethyl-formamide / 0.5 h / Cooling

4: toluene / 30 h / 120 °C

5: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 50 °C

6: triethylamine / dichloromethane / 1 h / 20 °C

7: sodium hydroxide / water / 20 °C

8: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 2 h

9: triethylamine / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; sodium azide; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; chloroformic acid ethyl ester; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c1cc11532d