succinic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester

Base Information

Chemical Name:succinic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester
CAS No.:309723-92-0
Molecular Formula:C₂₃H₂₂INO₆S
Molecular Weight:567.401
Hs Code.:

Synonyms:succinic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of succinic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester

Chemical Property:

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Technology Process of succinic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester

There total 4 articles about succinic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107-19-7
propargyl alcohol

: succinic acid mono-(2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl) ester

: 309723-92-0
succinic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester

Guidance literature:: With triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1016/S0040-4020(00)00660-8

Reference yield:

: 144863-34-3
3-(2'-iodo-N-phenylsulphonylanilinyl)-2-chloromethylpropene

: 309723-92-0
succinic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaOAc / dimethylformamide / 48 h / 80 °C

1.2: 78 percent / HCl / methanol / 24 h / 20 °C

2.1: DMAP; DCC / dimethylformamide / 12 h / 20 °C

3.1: triphenylphosphine; ADDP / tetrahydrofuran / 24 h / 20 °C

With dmap; sodium acetate; dicyclohexyl-carbodiimide; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; N,N-dimethyl-formamide; 1.1: Substitution / 1.2: Hydrolysis / 2.1: Etherification / 3.1: Etherification;
DOI:10.1016/S0040-4020(00)00660-8

Reference yield:

: sodium N-(2-iodophenyl)phenylsulfonamide

: 309723-92-0
succinic acid 2-{[benzenesulfonyl-(2-iodo-phenyl)-amino]-methyl}-allyl ester prop-2-ynyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethylformamide / 24 h

2.1: NaOAc / dimethylformamide / 48 h / 80 °C

2.2: 78 percent / HCl / methanol / 24 h / 20 °C

3.1: DMAP; DCC / dimethylformamide / 12 h / 20 °C

4.1: triphenylphosphine; ADDP / tetrahydrofuran / 24 h / 20 °C

With dmap; sodium acetate; dicyclohexyl-carbodiimide; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; N,N-dimethyl-formamide; 1.1: Substitution / 2.1: Substitution / 2.2: Hydrolysis / 3.1: Etherification / 4.1: Etherification;
DOI:10.1016/S0040-4020(00)00660-8