ethyl (2'S,3'S)-7-O-benzyl-6-O-chloroacetyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-L-glycero-α-D-manno-heptopyranoside

Base Information

Chemical Name:ethyl (2'S,3'S)-7-O-benzyl-6-O-chloroacetyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-L-glycero-α-D-manno-heptopyranoside
CAS No.:1169845-76-4
Molecular Formula:C₂₄H₃₅ClO₉S
Molecular Weight:535.056
Hs Code.:

Synonyms:ethyl (2'S,3'S)-7-O-benzyl-6-O-chloroacetyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-L-glycero-α-D-manno-heptopyranoside

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Chemical Property of ethyl (2'S,3'S)-7-O-benzyl-6-O-chloroacetyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-L-glycero-α-D-manno-heptopyranoside

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Technology Process of ethyl (2'S,3'S)-7-O-benzyl-6-O-chloroacetyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-L-glycero-α-D-manno-heptopyranoside

There total 1 articles about ethyl (2'S,3'S)-7-O-benzyl-6-O-chloroacetyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-L-glycero-α-D-manno-heptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 843674-49-7
ethyl (2'S,3'S)-7-O-benzyl-6-O-chloroacetyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-2-O-p-methoxybenzyl-1-thio-L-glycero-α-D-manno-heptopyranoside

: 1169845-76-4
ethyl (2'S,3'S)-7-O-benzyl-6-O-chloroacetyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 3h;
DOI:10.1016/j.tetasy.2009.02.017

Reference yield: 63.0%

: 1169845-76-4
ethyl (2'S,3'S)-7-O-benzyl-6-O-chloroacetyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-L-glycero-α-D-manno-heptopyranoside

: 145840-43-3
3,4,6-tri-O-acetyl-2-azido-2-deoxy-D-glucopyranosyl trichloroacetimidate

: 1169845-77-5
ethyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-glucopyranosyl-(1->2)-(2'S,3'S)-7-O-benzyl-6-O-chloroacetyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at 0 ℃; for 2.5h; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.02.017