(E)-3-phenyl-2-propenyl (E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl ether

Base Information

Chemical Name:(E)-3-phenyl-2-propenyl (E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl ether
CAS No.:1300748-80-4
Molecular Formula:C₃₄H₃₀N₂O
Molecular Weight:482.625
Hs Code.:

Synonyms:(E)-3-phenyl-2-propenyl (E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl ether

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Chemical Property of (E)-3-phenyl-2-propenyl (E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl ether

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Technology Process of (E)-3-phenyl-2-propenyl (E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl ether

There total 4 articles about (E)-3-phenyl-2-propenyl (E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 2687-12-9
cinnamyl chloride

: 199007-50-6
1-(1-Trityl-1H-imidazol4-yl)propen-3-ol

: 1300748-80-4
(E)-3-phenyl-2-propenyl (E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl ether

Guidance literature:: 1-(1-Trityl-1H-imidazol4-yl)propen-3-ol; With sodium hydride; In tetrahydrofuran; mineral oil; for 1h; Inert atmosphere; Cooling with ice;

cinnamyl chloride; In tetrahydrofuran; mineral oil; at 20 ℃; Inert atmosphere; Cooling with ice;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; mineral oil; at 20 ℃; Inert atmosphere;
DOI:10.1039/c0ob00657b

Reference yield:

: 112606-55-0
C₂₆H₂₂N₂O₂

: 1300748-80-4
(E)-3-phenyl-2-propenyl (E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisobutylaluminium hydride

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / Inert atmosphere; Cooling with ice

2.2: 20 °C / Inert atmosphere; Cooling with ice

2.3: 20 °C / Inert atmosphere

With sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1039/c0ob00657b

Reference yield:

: 104-98-3
urocanic acid

: 1300748-80-4
(E)-3-phenyl-2-propenyl (E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl ether

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid; magnesium sulfate / Reflux

2.1: triethylamine / N,N-dimethyl-formamide

3.1: diisobutylaluminium hydride

4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / Inert atmosphere; Cooling with ice

4.2: 20 °C / Inert atmosphere; Cooling with ice

4.3: 20 °C / Inert atmosphere

With sulfuric acid; sodium hydride; diisobutylaluminium hydride; magnesium sulfate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; 1.1: Fischer esterification;
DOI:10.1039/c0ob00657b