2,6-dimethyl-3,7-diphenyl-2,3,6,7-tetrahydrobenzo<1,2-d:4,5-d'>diisoxazole

Base Information

Chemical Name:2,6-dimethyl-3,7-diphenyl-2,3,6,7-tetrahydrobenzo<1,2-d:4,5-d'>diisoxazole
CAS No.:91477-76-8
Molecular Formula:C₂₂H₂₀N₂O₂
Molecular Weight:344.413
Hs Code.:

Synonyms:2,6-dimethyl-3,7-diphenyl-2,3,6,7-tetrahydrobenzo<1,2-d:4,5-d'>diisoxazole

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Chemical Property of 2,6-dimethyl-3,7-diphenyl-2,3,6,7-tetrahydrobenzo<1,2-d:4,5-d'>diisoxazole

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Technology Process of 2,6-dimethyl-3,7-diphenyl-2,3,6,7-tetrahydrobenzo<1,2-d:4,5-d'>diisoxazole

There total 2 articles about 2,6-dimethyl-3,7-diphenyl-2,3,6,7-tetrahydrobenzo<1,2-d:4,5-d'>diisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 3376-23-6,7372-59-0,59862-60-1
C-phenyl-N-methylnitrone

: 91477-70-2
1,5-diamino-1,5-dihydrobenzo<1,2-d:4,5-d'>bistriazole (DABT)

: 91477-76-8
2,6-dimethyl-3,7-diphenyl-2,3,6,7-tetrahydrobenzo<1,2-d:4,5-d'>diisoxazole

Guidance literature:: With lead(IV) acetate;
DOI:10.1016/S0040-4039(01)81164-3

Reference yield:

: 7221-63-8
1,5-dihydrobenzo<1,2-d:4,5-d'>bistriazole

: 91477-76-8
2,6-dimethyl-3,7-diphenyl-2,3,6,7-tetrahydrobenzo<1,2-d:4,5-d'>diisoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / KOH, NH₂OSO₃H / H₂O / 2 h / 60 °C

2: 91 percent / LTA

With lead(IV) acetate; potassium hydroxide; hydroxylamine-O-sulfonic acid; In water;
DOI:10.1016/S0040-4039(01)81164-3