ethyl (Z)-3-(furan-2-yl)-3-{[(trifluoromethyl)sulfonyl]-oxy}-2-propenoate

Base Information

Chemical Name:ethyl (Z)-3-(furan-2-yl)-3-{[(trifluoromethyl)sulfonyl]-oxy}-2-propenoate
CAS No.:288309-36-4
Molecular Formula:C₁₀H₉F₃O₆S
Molecular Weight:314.239
Hs Code.:

Synonyms:ethyl (Z)-3-(furan-2-yl)-3-{[(trifluoromethyl)sulfonyl]-oxy}-2-propenoate

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Chemical Property of ethyl (Z)-3-(furan-2-yl)-3-{[(trifluoromethyl)sulfonyl]-oxy}-2-propenoate

Chemical Property:

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Technology Process of ethyl (Z)-3-(furan-2-yl)-3-{[(trifluoromethyl)sulfonyl]-oxy}-2-propenoate

There total 1 articles about ethyl (Z)-3-(furan-2-yl)-3-{[(trifluoromethyl)sulfonyl]-oxy}-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 615-09-8
ethyl 3-(2-furyl)-3-oxopropanoate

: 358-23-6
trifluoromethylsulfonic anhydride

: 288309-36-4
ethyl (Z)-3-(furan-2-yl)-3-{[(trifluoromethyl)sulfonyl]-oxy}-2-propenoate

Guidance literature:: With triethylamine; In dichloromethane; at -78 ℃;
DOI:10.1016/S0960-894X(02)00199-3

Reference yield:

: 288309-36-4
ethyl (Z)-3-(furan-2-yl)-3-{[(trifluoromethyl)sulfonyl]-oxy}-2-propenoate

: 288309-38-6
(2E)-N-[4-(2-{[(tert-butyl)amino]sulfonyl}phenyl)phenyl]-3-(3-cyanophenyl)-3-(furan-2-yl)prop-2-enamide

Guidance literature:: Multi-step reaction with 2 steps

1: Pd(Ph₃P)4; K₃PO₄ / dioxane / Heating

2: AlMe₃ / CH₂Cl₂

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trimethylaluminum; In 1,4-dioxane; dichloromethane; 2: Weinreb amidation;
DOI:10.1016/S0960-894X(02)00199-3

Reference yield:

: 288309-36-4
ethyl (Z)-3-(furan-2-yl)-3-{[(trifluoromethyl)sulfonyl]-oxy}-2-propenoate

: 3-((1E)-1-(furan-2-yl)-2-{N-[4-(2-sulfamoylphenyl)phenyl]carbamoyl}vinyl)benzenecarboxamidine

Guidance literature:: Multi-step reaction with 4 steps

1: Pd(Ph₃P)4; K₃PO₄ / dioxane / Heating

2: AlMe₃ / CH₂Cl₂

3: HCl(g); MeOH

4: NH₄OAc

With hydrogenchloride; methanol; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium acetate; trimethylaluminum; In 1,4-dioxane; dichloromethane; 2: Weinreb amidation / 3: Pinner reaction;
DOI:10.1016/S0960-894X(02)00199-3