N-<4-(phenylsulfonyl)benzyl>-N-methyl-6-aminobenzindol-2(1H)-thione

Base Information

Chemical Name:N-<4-(phenylsulfonyl)benzyl>-N-methyl-6-aminobenzindol-2(1H)-thione
CAS No.:138385-07-6
Molecular Formula:C₂₅H₂₀N₂O₂S₂
Molecular Weight:444.578
Hs Code.:

N-<4-(phenylsulfonyl)benzyl>-N-methyl-6-aminobenz<cd>indol-2(1H)-thione

Synonyms:N-<4-(phenylsulfonyl)benzyl>-N-methyl-6-aminobenzindol-2(1H)-thione

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Chemical Property of N-<4-(phenylsulfonyl)benzyl>-N-methyl-6-aminobenzindol-2(1H)-thione

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Technology Process of N-<4-(phenylsulfonyl)benzyl>-N-methyl-6-aminobenzindol-2(1H)-thione

There total 10 articles about N-<4-(phenylsulfonyl)benzyl>-N-methyl-6-aminobenzindol-2(1H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 138384-72-2
N⁶-<4-(phenylsulfonyl)benzyl>-N⁶-methyl-6-aminobenzindol-2(1H)-one

: 138385-07-6
N-<4-(phenylsulfonyl)benzyl>-N-methyl-6-aminobenzindol-2(1H)-thione

Guidance literature:: With Lawessons reagent; In toluene; at 120 ℃; for 1h;
DOI:10.1021/jm00082a006

Reference yield:

: 130-00-7
1,8-naphtholactam

: 138385-07-6
N-<4-(phenylsulfonyl)benzyl>-N-methyl-6-aminobenzindol-2(1H)-thione

Guidance literature:: Multi-step reaction with 5 steps

1: 51 percent / 70percent HNO₃ / acetic acid / 1 h / 20 - 50 °C

2: H₂ / 5percent Pd/C / tetrahydrofuran / 16 h / 2068.6 Torr

3: 71 percent / DIEA / dimethylformamide / 3 h / 75 °C

4: 26 percent / DIEA / dimethylformamide / 19 h / 95 °C

5: 47 percent / Lawesson's reagent / toluene / 1 h / 120 °C

With Lawessons reagent; hydrogen; nitric acid; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00082a006

Reference yield:

: 65300-66-5
N-(2,4-dinitrophenoxy)-4-nitronaphthalimide

: 138385-07-6
N-<4-(phenylsulfonyl)benzyl>-N-methyl-6-aminobenzindol-2(1H)-thione

Guidance literature:: Multi-step reaction with 5 steps

1: NaOH / ethanol; H₂O / 16 h / 25 °C

2: H₂ / 5percent Pd/C / tetrahydrofuran / 16 h / 2068.6 Torr

3: 71 percent / DIEA / dimethylformamide / 3 h / 75 °C

4: 26 percent / DIEA / dimethylformamide / 19 h / 95 °C

5: 47 percent / Lawesson's reagent / toluene / 1 h / 120 °C

With Lawessons reagent; sodium hydroxide; hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00082a006