2-amino-7-(2-deoxy-2-fluoro-3,5-di-O-benzoyl-β-D-arabinofuranosyl)-5,6-dihydropyrrolo<2,3-d>pyrimidine

Base Information

Chemical Name:2-amino-7-(2-deoxy-2-fluoro-3,5-di-O-benzoyl-β-D-arabinofuranosyl)-5,6-dihydropyrrolo<2,3-d>pyrimidine
CAS No.:170468-50-5
Molecular Formula:C₂₅H₂₃FN₄O₅
Molecular Weight:478.48
Hs Code.:

Synonyms:2-amino-7-(2-deoxy-2-fluoro-3,5-di-O-benzoyl-β-D-arabinofuranosyl)-5,6-dihydropyrrolo<2,3-d>pyrimidine

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Chemical Property of 2-amino-7-(2-deoxy-2-fluoro-3,5-di-O-benzoyl-β-D-arabinofuranosyl)-5,6-dihydropyrrolo<2,3-d>pyrimidine

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Technology Process of 2-amino-7-(2-deoxy-2-fluoro-3,5-di-O-benzoyl-β-D-arabinofuranosyl)-5,6-dihydropyrrolo<2,3-d>pyrimidine

There total 3 articles about 2-amino-7-(2-deoxy-2-fluoro-3,5-di-O-benzoyl-β-D-arabinofuranosyl)-5,6-dihydropyrrolo<2,3-d>pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 170468-33-4
2-amino-4-chloro-7-(2-deoxy-2-fluoro-3,5-di-O-benzoyl-β-D-arabinofuranosyl)pyrrolo<2,3-d>pyrimidine

: 170468-50-5
2-amino-7-(2-deoxy-2-fluoro-3,5-di-O-benzoyl-β-D-arabinofuranosyl)-5,6-dihydropyrrolo<2,3-d>pyrimidine

Guidance literature:: With ammonium formate; palladium on activated charcoal; In methanol; for 2h; Heating;
DOI:10.1021/jm00020a009

Reference yield:

: 97614-44-3
2-deoxy-2-fluoro-3,5-di-O-benzoyl-α-D-arabinofuranosyl bromide

: 170468-50-5
2-amino-7-(2-deoxy-2-fluoro-3,5-di-O-benzoyl-β-D-arabinofuranosyl)-5,6-dihydropyrrolo<2,3-d>pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) CH₃CN, RT, 1 H, 2.) CH₃CN, RT, 24 h

2: 75 percent / ammonium formate / 10percent Pd/C / methanol / 2 h / Heating

With ammonium formate; sodium hydride; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00020a009

Reference yield:

: 84955-31-7
4-chloro-7H-pyrrolo[2,3-d]pyrimidin-2-amine

: 170468-50-5
2-amino-7-(2-deoxy-2-fluoro-3,5-di-O-benzoyl-β-D-arabinofuranosyl)-5,6-dihydropyrrolo<2,3-d>pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) CH₃CN, RT, 1 H, 2.) CH₃CN, RT, 24 h

2: 75 percent / ammonium formate / 10percent Pd/C / methanol / 2 h / Heating

With ammonium formate; sodium hydride; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00020a009