bis(phenylethynyl)zirkonocene

Base Information

Chemical Name:bis(phenylethynyl)zirkonocene
CAS No.:72982-57-1
Molecular Formula:C₂₆H₂₀Zr
Molecular Weight:423.669
Hs Code.:

Synonyms:bis(phenylethynyl)zirkonocene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(phenylethynyl)zirkonocene

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Technology Process of bis(phenylethynyl)zirkonocene

There total 3 articles about bis(phenylethynyl)zirkonocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.7%

: bis(dimethylamino)zirconocene

: 536-74-3
phenylacetylene

: 72982-57-1
bis(phenylethynyl)zirkonocene

Guidance literature:: In tetrahydrofuran; (π-C5H5)ZrCl2/C6H5CCH (molar ratio: 1:2); reflux (1 h);;
DOI:10.1016/S0022-328X(00)92810-9

Reference yield: 64.0%

: 1291-32-3
zirconocene dichloride

: 4440-01-1
lithium phenylacetylide

: 72982-57-1
bis(phenylethynyl)zirkonocene

Guidance literature:: In benzene; in darkness, 2.equiv. of LiCCPh, stirred for 24 h;
DOI:10.1039/b004478o

Reference yield: 61.0%

: 1291-32-3
zirconocene dichloride

: 1004-22-4
phenylethynylsodium

: 72982-57-1
bis(phenylethynyl)zirkonocene

Guidance literature:: In diethyl ether; byproducts: NaCl; suspn. in ether stirred (5 h, room temp., Ar); evapd. (vac.), residue extd. with benzene, filtered, evapd., pentane added; elem. anal.;