methyl (2S,3'R)-2-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-4-methylpentanoate

Base Information

Chemical Name:methyl (2S,3'R)-2-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-4-methylpentanoate
CAS No.:797049-78-6
Molecular Formula:C₂₁H₃₂N₂O₅
Molecular Weight:392.495
Hs Code.:

Synonyms:methyl (2S,3'R)-2-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-4-methylpentanoate

Suppliers and Price of methyl (2S,3'R)-2-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-4-methylpentanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of methyl (2S,3'R)-2-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-4-methylpentanoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of methyl (2S,3'R)-2-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-4-methylpentanoate

There total 2 articles about methyl (2S,3'R)-2-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-4-methylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2666-93-5
(S)-Leu-OMe

: 215608-32-5
(R)-3-<(benzyoxycarbonyl)amino>-4-methylpentanoic acid

: 797049-78-6
methyl (2S,3'R)-2-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-4-methylpentanoate

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1071/CH04080

Reference yield:

: 112121-72-9
Methyl (R)-(-)-N-benzyloxycarbonylamino-4-methylpentanoate

: 797049-78-6
methyl (2S,3'R)-2-(3-benzyloxycarbonylamino-4-methylpentanoylamino)-4-methylpentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / tetrahydrofuran; H₂O / 3 h / 40 °C

2: 100 percent / BOP; iPr₂NEt / CH₂Cl₂

With potassium hydroxide; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1071/CH04080