2-(3-(3,4-dichlorobenzyl)-4-oxo-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-6-ylamino)-2-oxoethyl acetate

Base Information

Chemical Name:2-(3-(3,4-dichlorobenzyl)-4-oxo-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-6-ylamino)-2-oxoethyl acetate
CAS No.:1190093-11-8
Molecular Formula:C₁₇H₁₄Cl₂N₄O₄
Molecular Weight:409.229
Hs Code.:

Synonyms:2-(3-(3,4-dichlorobenzyl)-4-oxo-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-6-ylamino)-2-oxoethyl acetate

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Chemical Property of 2-(3-(3,4-dichlorobenzyl)-4-oxo-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-6-ylamino)-2-oxoethyl acetate

Chemical Property:

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Technology Process of 2-(3-(3,4-dichlorobenzyl)-4-oxo-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-6-ylamino)-2-oxoethyl acetate

There total 6 articles about 2-(3-(3,4-dichlorobenzyl)-4-oxo-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-6-ylamino)-2-oxoethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5930-93-8
4-nitropyrrole-2-carboxylic acid

: 1190093-11-8
2-(3-(3,4-dichlorobenzyl)-4-oxo-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-6-ylamino)-2-oxoethyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 2 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C

2.2: 0 - 20 °C

3.1: pyridinium p-toluenesulfonate / 3 h / Reflux

4.1: hydrazine hydrate / nickel / methanol; water / Reflux

5.1: triethylamine / dichloromethane / 1 h / 20 °C

With sodium hydride; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; pyridinium p-toluenesulfonate; nickel; In methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1190093-60-7
6-amino-3-(3,4-dichlorobenzyl)pyrrolo[1,2-f][1,2,4]triazin-4(3H)-one

: 13831-31-7
Acetoxyacetyl chloride

: 1190093-11-8
2-(3-(3,4-dichlorobenzyl)-4-oxo-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-6-ylamino)-2-oxoethyl acetate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 1190093-47-0
1-amino-N-(3,4-dichlorobenzyl)-4-nitro-1-pyrrole-2-carboxamide

: 1190093-11-8
2-(3-(3,4-dichlorobenzyl)-4-oxo-3,4-dihydropyrrolo[1,2-f][1,2,4]triazin-6-ylamino)-2-oxoethyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium p-toluenesulfonate / 3 h / Reflux

2: hydrazine hydrate / nickel / methanol; water / Reflux

3: triethylamine / dichloromethane / 1 h / 20 °C

With hydrazine hydrate; triethylamine; pyridinium p-toluenesulfonate; nickel; In methanol; dichloromethane; water;