allyl 6-O-benzyl-4-O-benzyloxycarbonylmethyl-3-O-((R)-3-benzyloxytetradecanoyl)-2-deoxy-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

Base Information

Chemical Name:allyl 6-O-benzyl-4-O-benzyloxycarbonylmethyl-3-O-((R)-3-benzyloxytetradecanoyl)-2-deoxy-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside
CAS No.:927175-32-4
Molecular Formula:C₄₉H₆₄Cl₃NO₁₁
Molecular Weight:949.406
Hs Code.:

allyl 6-O-benzyl-4-O-benzyloxycarbonylmethyl-3-O-((R)-3-benzyloxytetradecanoyl)-2-deoxy-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

Synonyms:allyl 6-O-benzyl-4-O-benzyloxycarbonylmethyl-3-O-((R)-3-benzyloxytetradecanoyl)-2-deoxy-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

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Chemical Property of allyl 6-O-benzyl-4-O-benzyloxycarbonylmethyl-3-O-((R)-3-benzyloxytetradecanoyl)-2-deoxy-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

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Technology Process of allyl 6-O-benzyl-4-O-benzyloxycarbonylmethyl-3-O-((R)-3-benzyloxytetradecanoyl)-2-deoxy-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

There total 3 articles about allyl 6-O-benzyl-4-O-benzyloxycarbonylmethyl-3-O-((R)-3-benzyloxytetradecanoyl)-2-deoxy-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 81867-37-0
benzyl iodoacetate

: 185801-05-2
allyl 6-O-benzyl-3-O-[(R)-3-(benzyloxy)tetradecanoyl]-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

: 927175-32-4
allyl 6-O-benzyl-4-O-benzyloxycarbonylmethyl-3-O-((R)-3-benzyloxytetradecanoyl)-2-deoxy-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; silver(l) oxide; In toluene; at 20 ℃; for 240h;
DOI:10.3987/com-06-s(o)51

Reference yield:

: allyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

: 927175-32-4
allyl 6-O-benzyl-4-O-benzyloxycarbonylmethyl-3-O-((R)-3-benzyloxytetradecanoyl)-2-deoxy-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / triethylsilane; boron trifluoride diethyl etherate / CH₂Cl₂ / 5 h / 20 °C

2: 79 percent / silver oxide; 4 Angstroem molecular sieves / toluene / 240 h / 20 °C

With triethylsilane; 4 A molecular sieve; boron trifluoride diethyl etherate; silver(l) oxide; In dichloromethane; toluene;
DOI:10.3987/com-06-s(o)51

Reference yield:

: allyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

: 927175-32-4
allyl 6-O-benzyl-4-O-benzyloxycarbonylmethyl-3-O-((R)-3-benzyloxytetradecanoyl)-2-deoxy-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / DMAP; DCC / CH₂Cl₂ / 2 h / 20 °C

2: 85 percent / triethylsilane; boron trifluoride diethyl etherate / CH₂Cl₂ / 5 h / 20 °C

3: 79 percent / silver oxide; 4 Angstroem molecular sieves / toluene / 240 h / 20 °C

With triethylsilane; dmap; 4 A molecular sieve; boron trifluoride diethyl etherate; dicyclohexyl-carbodiimide; silver(l) oxide; In dichloromethane; toluene;
DOI:10.3987/com-06-s(o)51