N-[3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-4-[(trifluoromethyl)-sulfinyl]-1H-pyrazol-5-yl]-aminoethanol

Base Information

Chemical Name:N-[3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-4-[(trifluoromethyl)-sulfinyl]-1H-pyrazol-5-yl]-aminoethanol
CAS No.:1430089-23-8
Molecular Formula:C₁₄H₈Cl₂F₆N₄O₂S
Molecular Weight:481.206
Hs Code.:

Synonyms:N-[3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-4-[(trifluoromethyl)-sulfinyl]-1H-pyrazol-5-yl]-aminoethanol

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Chemical Property of N-[3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-4-[(trifluoromethyl)-sulfinyl]-1H-pyrazol-5-yl]-aminoethanol

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Technology Process of N-[3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-4-[(trifluoromethyl)-sulfinyl]-1H-pyrazol-5-yl]-aminoethanol

There total 2 articles about N-[3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-4-[(trifluoromethyl)-sulfinyl]-1H-pyrazol-5-yl]-aminoethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1430089-22-7
ethyl N-[3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-4-[(trifluoromethyl)-sulfinyl]-1H-pyrazol-5-yl]-aminoacetate

: 1430089-23-8
N-[3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-4-[(trifluoromethyl)-sulfinyl]-1H-pyrazol-5-yl]-aminoethanol

Guidance literature:: With sodium tetrahydroborate; zinc(II) chloride; In tetrahydrofuran; at 50 ℃; for 1h;
DOI:10.1021/jf400888c

Reference yield:

: 120068-37-3
fipronil

: 1430089-23-8
N-[3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-4-[(trifluoromethyl)-sulfinyl]-1H-pyrazol-5-yl]-aminoethanol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran / 3 h / 20 °C / Cooling with ice

2: sodium tetrahydroborate; zinc(II) chloride / tetrahydrofuran / 1 h / 50 °C

With sodium tetrahydroborate; sodium hydride; zinc(II) chloride; In tetrahydrofuran;
DOI:10.1021/jf400888c

Reference yield:

: 1430089-23-8
N-[3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-4-[(trifluoromethyl)-sulfinyl]-1H-pyrazol-5-yl]-aminoethanol

: 128377-34-4,869848-87-3
2,3,4-tri-O-acetyl-β-D-xylopyranoside trichloroacetimidate

: C₂₅H₂₂Cl₂F₆N₄O₉S

Guidance literature:: N-[3-cyano-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-4-[(trifluoromethyl)-sulfinyl]-1H-pyrazol-5-yl]-aminoethanol; 2,3,4-tri-O-acetyl-β-D-xylopyranoside trichloroacetimidate; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve;

With boron trifluoride diethyl etherate; In dichloromethane; at -30 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/jf400888c