2,4-di-O-benzoyl-3-O-benzyl-6-O-trityl-α-D-glucopyranosyl trichloroacetimidate

Base Information

• Chemical Name: 2,4-di-O-benzoyl-3-O-benzyl-6-O-trityl-α-D-glucopyranosyl trichloroacetimidate
• CAS No.: 1039373-56-2
• Molecular Formula: C₄₈H₄₀Cl₃NO₈
• Molecular Weight: 865.207

Synonyms:2,4-di-O-benzoyl-3-O-benzyl-6-O-trityl-α-D-glucopyranosyl trichloroacetimidate

Chemical Property of 2,4-di-O-benzoyl-3-O-benzyl-6-O-trityl-α-D-glucopyranosyl trichloroacetimidate

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Technology Process of 2,4-di-O-benzoyl-3-O-benzyl-6-O-trityl-α-D-glucopyranosyl trichloroacetimidate

There total 1 articles about 2,4-di-O-benzoyl-3-O-benzyl-6-O-trityl-α-D-glucopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C46H40O8 + trichloroacetonitrile (545-06-2) → 2,4-di-O-benzoyl-3-O-benzyl-6-O-trityl-α-D-glucopyranosyl trichloroacetimidate (1039373-56-2)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/jo800669h

Reference yield: 95.0%

2,4-di-O-benzoyl-3-O-benzyl-6-O-trityl-α-D-glucopyranosyl trichloroacetimidate (1039373-56-2) + acetic acid (64-19-7,77671-22-8) → 1-O-acetyl-2,4-di-O-benzoyl-3-O-benzyl-6-O-trityl-β-D-glucopyranoside (1039373-95-9)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/jo800669h

Reference yield: 92.0%

2,4-di-O-benzoyl-3-O-benzyl-6-O-trityl-α-D-glucopyranosyl trichloroacetimidate (1039373-56-2) + oleanolic acid 28-O-2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl ester (676530-80-6) → 28-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)oleanate 3-O-(2,4-di-O-benzoyl-3-O-benzyl-6-O-trityl-β-D-glucopyranoside) (1039373-70-0)

Guidance literature:

With t-butyldimethylsiyl triflate; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/jo800669h

upstream raw materials:

trichloroacetonitrile

Downstream raw materials:

1-O-acetyl-2,4-di-O-benzoyl-3-O-benzyl-6-O-trityl-β-D-glucopyranoside

28-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)oleanate 3-O-(2,4-di-O-benzoyl-3-O-benzyl-6-O-trityl-β-D-glucopyranoside)

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