{(4S,5R)-2,2-Dimethyl-5-[(S)-phenylsulfanyl-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-methyl]-[1,3]dioxolan-4-yl}-methanol

Base Information

Chemical Name:{(4S,5R)-2,2-Dimethyl-5-[(S)-phenylsulfanyl-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-methyl]-[1,3]dioxolan-4-yl}-methanol
CAS No.:84034-53-7
Molecular Formula:C₄₁H₄₈O₉S
Molecular Weight:716.893
Hs Code.:

{(4S,5R)-2,2-Dimethyl-5-[(S)-phenylsulfanyl-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-methyl]-[1,3]dioxolan-4-yl}-methanol

Synonyms:{(4S,5R)-2,2-Dimethyl-5-[(S)-phenylsulfanyl-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-methyl]-[1,3]dioxolan-4-yl}-methanol

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Chemical Property of {(4S,5R)-2,2-Dimethyl-5-[(S)-phenylsulfanyl-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-methyl]-[1,3]dioxolan-4-yl}-methanol

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Technology Process of {(4S,5R)-2,2-Dimethyl-5-[(S)-phenylsulfanyl-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-methyl]-[1,3]dioxolan-4-yl}-methanol

There total 1 articles about {(4S,5R)-2,2-Dimethyl-5-[(S)-phenylsulfanyl-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-methyl]-[1,3]dioxolan-4-yl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 84034-50-4
(4R,5R)-2,2-Dimethyl-5-[(S)-phenylsulfanyl-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-methyl]-[1,3]dioxolane-4-carboxylic acid methyl ester

: 84034-53-7
{(4S,5R)-2,2-Dimethyl-5-[(S)-phenylsulfanyl-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-methyl]-[1,3]dioxolan-4-yl}-methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1246/cl.1982.1555

Reference yield: 66.0%

: 84034-53-7
{(4S,5R)-2,2-Dimethyl-5-[(S)-phenylsulfanyl-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-methyl]-[1,3]dioxolan-4-yl}-methanol

: 84034-57-1
(2S,3R,4S)-4-Phenylsulfanyl-4-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-butane-1,2,3-triol

Guidance literature:: With hydrogenchloride; In methanol; water; Ambient temperature;
DOI:10.1246/cl.1982.1555

Reference yield:

: 84034-53-7
{(4S,5R)-2,2-Dimethyl-5-[(S)-phenylsulfanyl-((2R,3R,4S,5R,6S)-3,4,5-tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-methyl]-[1,3]dioxolan-4-yl}-methanol

: 84034-60-6
(2R,3R,4S)-2-((2R,3R,4S,5R,6S)-3,4,5-Tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-furan-3,4-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / 2N HCl / methanol; H₂O / Ambient temperature

2: 76 percent / HgCl₂/HgO / 1,2-dimethoxy-ethane; H₂O / 1.5 h / Ambient temperature

With hydrogenchloride; mercury dichloride; mercury(II) oxide; In methanol; 1,2-dimethoxyethane; water;
DOI:10.1246/cl.1982.1555