C₃₁H₃₆O₁₁

Base Information

Chemical Name:C₃₁H₃₆O₁₁
CAS No.:861114-12-7
Molecular Formula:C₃₁H₃₆O₁₁
Molecular Weight:584.62
Hs Code.:

C<sub>31</sub>H<sub>36</sub>O<sub>11</sub>

Synonyms:C₃₁H₃₆O₁₁

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Chemical Property of C₃₁H₃₆O₁₁

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Technology Process of C₃₁H₃₆O₁₁

There total 21 articles about C₃₁H₃₆O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 861113-97-5
C₃₈H₅₇F₃O₁₄SSi₂

: 861114-12-7
C₃₁H₃₆O₁₁

Guidance literature:: Multi-step reaction with 14 steps

1.1: 95 percent / Et₃SiH; Pd(PPh₃)4; LiCl / dimethylformamide / 24 h / 55 °C

2.1: 96 percent / K₂OsO₄*2H₂O; (DHQD)2PHAL; MeSO₂NH₂ / K₃Fe(CN)6; K₂CO₃ / 2-methyl-propan-2-ol; H₂O / 2 h

3.1: 98 percent / Et₃N; DMAP / CH₂Cl₂ / 8 h / 0 - 25 °C

4.1: H₂ / Pd(OH)2/C / methanol; H₂O / 2 h / 25 °C / pH 7

5.1: base

6.1: NaBH₄ / methanol / 0.5 h / 0 - 25 °C

7.1: Pb(OAc)4 / CH₂Cl₂ / 2 h / 0 - 25 °C

8.1: 70 percent / DBU / toluene / 4 h / Heating

9.1: SOCl₂; pyridine / 8 h / 0 - 25 °C

9.2: K₂CO₃; MeOH / 2 h / 25 °C

10.1: Br₂; N,N-dimethylaniline; K₂CO₃ / CH₂Cl₂ / 0.17 h / -78 °C

10.2: 76 percent / N,N-dimethylaniline; K₂CO₃ / CH₂Cl₂ / 3 h / -78 - 0 °C

11.1: 42 percent / (Me₃Si)3SiH; AIBN / toluene / 0.5 h / 110 °C

12.1: 88 percent / NaBH₄ / methanol / 0.25 h / 0 °C

13.1: pyridine; DMAP / 5 h / 60 °C

14.1: HCl / methanol; diethyl ether / 4 h / 0 - 25 °C

With pyridine; lead(IV) acetate; hydrogenchloride; triethylsilane; dmap; sodium tetrahydroborate; potassium osmate(VI); tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; 2,2'-azobis(isobutyronitrile); methanesulfonamide; tris-(trimethylsilyl)silane; hydrogen; bromine; potassium carbonate; N,N-dimethyl-aniline; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; lithium chloride; palladium dihydroxide; potassium carbonate; potassium hexacyanoferrate(III); In methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1002/anie.200500217

Reference yield:

: 861113-99-7
C₃₇H₆₀O₁₃Si₂

: 861114-12-7
C₃₁H₃₆O₁₁

Guidance literature:: Multi-step reaction with 12 steps

1.1: 98 percent / Et₃N; DMAP / CH₂Cl₂ / 8 h / 0 - 25 °C

2.1: H₂ / Pd(OH)2/C / methanol; H₂O / 2 h / 25 °C / pH 7

3.1: base

4.1: NaBH₄ / methanol / 0.5 h / 0 - 25 °C

5.1: Pb(OAc)4 / CH₂Cl₂ / 2 h / 0 - 25 °C

6.1: 70 percent / DBU / toluene / 4 h / Heating

7.1: SOCl₂; pyridine / 8 h / 0 - 25 °C

7.2: K₂CO₃; MeOH / 2 h / 25 °C

8.1: Br₂; N,N-dimethylaniline; K₂CO₃ / CH₂Cl₂ / 0.17 h / -78 °C

8.2: 76 percent / N,N-dimethylaniline; K₂CO₃ / CH₂Cl₂ / 3 h / -78 - 0 °C

9.1: 42 percent / (Me₃Si)3SiH; AIBN / toluene / 0.5 h / 110 °C

10.1: 88 percent / NaBH₄ / methanol / 0.25 h / 0 °C

11.1: pyridine; DMAP / 5 h / 60 °C

12.1: HCl / methanol; diethyl ether / 4 h / 0 - 25 °C

With pyridine; lead(IV) acetate; hydrogenchloride; dmap; sodium tetrahydroborate; thionyl chloride; 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; hydrogen; bromine; potassium carbonate; N,N-dimethyl-aniline; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; palladium dihydroxide; In methanol; diethyl ether; dichloromethane; water; toluene;
DOI:10.1002/anie.200500217

Reference yield:

: 861114-00-3
C₃₉H₆₂O₁₄Si₂

: 861114-12-7
C₃₁H₃₆O₁₁

Guidance literature:: Multi-step reaction with 11 steps

1.1: H₂ / Pd(OH)2/C / methanol; H₂O / 2 h / 25 °C / pH 7

2.1: base

3.1: NaBH₄ / methanol / 0.5 h / 0 - 25 °C

4.1: Pb(OAc)4 / CH₂Cl₂ / 2 h / 0 - 25 °C

5.1: 70 percent / DBU / toluene / 4 h / Heating

6.1: SOCl₂; pyridine / 8 h / 0 - 25 °C

6.2: K₂CO₃; MeOH / 2 h / 25 °C

7.1: Br₂; N,N-dimethylaniline; K₂CO₃ / CH₂Cl₂ / 0.17 h / -78 °C

7.2: 76 percent / N,N-dimethylaniline; K₂CO₃ / CH₂Cl₂ / 3 h / -78 - 0 °C

8.1: 42 percent / (Me₃Si)3SiH; AIBN / toluene / 0.5 h / 110 °C

9.1: 88 percent / NaBH₄ / methanol / 0.25 h / 0 °C

10.1: pyridine; DMAP / 5 h / 60 °C

11.1: HCl / methanol; diethyl ether / 4 h / 0 - 25 °C

With pyridine; lead(IV) acetate; hydrogenchloride; dmap; sodium tetrahydroborate; thionyl chloride; 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; hydrogen; bromine; potassium carbonate; N,N-dimethyl-aniline; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium dihydroxide; In methanol; diethyl ether; dichloromethane; water; toluene;
DOI:10.1002/anie.200500217