C₁₃₂H₁₉₈O₆₀

Base Information

• Chemical Name: C₁₃₂H₁₉₈O₆₀
• CAS No.: 1133232-94-6
• Molecular Formula: C₁₃₂H₁₉₈O₆₀
• Molecular Weight: 2744.99
• Mol file: 1133232-94-6.mol

Synonyms:C₁₃₂H₁₉₈O₆₀

Chemical Property of C₁₃₂H₁₉₈O₆₀

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₁₃₂H₁₉₈O₆₀

There total 2 articles about C₁₃₂H₁₉₈O₆₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

C138H214O60Si2 (1133232-93-5) → C132H198O60 (1133232-94-6)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1016/j.tetlet.2008.12.087

Reference yield: 84.0%

4-(trimethylsilylethynyl)phenylacetylene (66228-76-0) + 2,5-diiodo-1,4-hydroquinone (13064-64-7) + 6-O-monotosyl permethylated α-cyclodextrin (94789-62-5) → C132H198O60 (1133232-94-6)

Guidance literature:

2,5-diiodo-1,4-hydroquinone; 6-O-monotosyl permethylated α-cyclodextrin; With potassium carbonate; In N,N-dimethyl-formamide; Inert atmosphere; Schlenk technique;

4-(trimethylsilylethynyl)phenylacetylene; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; Inert atmosphere; Schlenk technique;

With potassium carbonate; In methanol; Inert atmosphere; Schlenk technique;

DOI:10.1002/anie.201603160

Reference yield: 90.0%

C132H198O60 (1133232-94-6) + 1-(4-iodophenyl)-2-(tert-butyldimethylsilyl)acetylene (1514901-78-0) → C160H234O60Si2

Guidance literature:

With copper(l) iodide; palladium diacetate; caesium carbonate; triethylamine; tris(4,6-dimethyl-3-sulfonatophenyl)phosphine trisodium salt hydrate; In methanol; water; at 50 ℃; for 16h; Inert atmosphere;

DOI:10.1021/ja508636z

upstream raw materials:

C₁₃₈H₂₁₄O₆₀Si₂

4-(trimethylsilylethynyl)phenylacetylene

2,5-diiodo-1,4-hydroquinone

6-O-monotosyl permethylated α-cyclodextrin

Downstream raw materials:

C₁₅₂H₂₂₂O₆₀

C₁₄₆H₂₀₈N₆O₆₄