(2S,3R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2,3-dimethyl-5-oxo-2,3,4,5-tetrahydrofuran-2-carboxylate

Base Information

Chemical Name:(2S,3R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2,3-dimethyl-5-oxo-2,3,4,5-tetrahydrofuran-2-carboxylate
CAS No.:139944-72-2
Molecular Formula:C₂₃H₃₂O₄
Molecular Weight:372.505
Hs Code.:

Synonyms:(2S,3R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2,3-dimethyl-5-oxo-2,3,4,5-tetrahydrofuran-2-carboxylate

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Chemical Property of (2S,3R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2,3-dimethyl-5-oxo-2,3,4,5-tetrahydrofuran-2-carboxylate

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Technology Process of (2S,3R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2,3-dimethyl-5-oxo-2,3,4,5-tetrahydrofuran-2-carboxylate

There total 6 articles about (2S,3R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2,3-dimethyl-5-oxo-2,3,4,5-tetrahydrofuran-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 139944-76-6
5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2,5-dihydro-2,3-dimethyl-5-oxofuran-2-carboxylate

: 139944-72-2
(2S,3R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2,3-dimethyl-5-oxo-2,3,4,5-tetrahydrofuran-2-carboxylate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 6h; under 760 Torr; Ambient temperature;
DOI:10.1021/jo00036a034

Reference yield:

: 65253-04-5
(-)-8-phenylmenthol

: 139944-72-2
(2S,3R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2,3-dimethyl-5-oxo-2,3,4,5-tetrahydrofuran-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent

3: water, HgCl₂ / methanol / 5 h / Heating

With water; mercury dichloride; In methanol;
DOI:10.1021/jo00036a034

Reference yield:

: 88292-41-5
2-Oxopropansaeure-<(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl>ester

: 139944-72-2
(2S,3R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2,3-dimethyl-5-oxo-2,3,4,5-tetrahydrofuran-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

2: water, HgCl₂ / methanol / 5 h / Heating

With water; mercury dichloride; In methanol;
DOI:10.1021/jo00036a034