C₇₀H₈₆N₆O₁₀

Base Information

• Chemical Name: C₇₀H₈₆N₆O₁₀
• CAS No.: 1616282-98-4
• Molecular Formula: C₇₀H₈₆N₆O₁₀
• Molecular Weight: 1171.49
• Mol file: 1616282-98-4.mol

Synonyms:C₇₀H₈₆N₆O₁₀

Chemical Property of C₇₀H₈₆N₆O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₇₀H₈₆N₆O₁₀

There total 5 articles about C₇₀H₈₆N₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

C71H86N6O11 (1616282-97-3) → C70H86N6O10 (1616282-98-4)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1021/ja5041573

Reference yield:

C21H28N2O3 (1575790-50-9) → C70H86N6O10 (1616282-98-4)

Guidance literature:

Multi-step reaction with 3 steps

1: phosphorus tribromide / N,N-dimethyl-formamide; dichloromethane; tetrahydrofuran / 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 70 °C / Inert atmosphere

3: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; phosphorus tribromide; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja5041573

Reference yield:

C21H27BrN2O2 (149474-78-2) → C70H86N6O10 (1616282-98-4)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 70 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1021/ja5041573

upstream raw materials:

C₇₁H₈₆N₆O₁₁

(E)-4-hydroxy-4′-methoxyazobenzene

C₂₁H₂₈N₂O₃

C₂₁H₂₇BrN₂O₂

Downstream raw materials:

C₇₀H₈₅ClN₆O₉

Refernces