2-hydroxymethylbutyl phenyl sulfide

Base Information

• Chemical Name: 2-hydroxymethylbutyl phenyl sulfide
• CAS No.: 1246953-28-5
• Molecular Formula: C₁₁H₁₆OS
• Molecular Weight: 196.313
• Mol file: 1246953-28-5.mol

Synonyms:2-hydroxymethylbutyl phenyl sulfide

Chemical Property of 2-hydroxymethylbutyl phenyl sulfide

Chemical Property:

Purity/Quality:

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Technology Process of 2-hydroxymethylbutyl phenyl sulfide

There total 1 articles about 2-hydroxymethylbutyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2-(acetoxymethyl)butyl methanesulfonate (1246953-25-2) + thiophenol (108-98-5) → 2-hydroxymethylbutyl phenyl sulfide (1246953-28-5)

Guidance literature:

thiophenol; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.25h;

2-(acetoxymethyl)butyl methanesulfonate; In tetrahydrofuran; mineral oil; at 50 ℃;

DOI:10.1002/ejoc.201000539

Reference yield: 89.0%

2-hydroxymethylbutyl phenyl sulfide (1246953-28-5) → (R)-2-((phenylsulfonyl)methyl)butan-1-ol (1246953-38-7)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃;

DOI:10.1002/ejoc.201000539

upstream raw materials:

2-(acetoxymethyl)butyl methanesulfonate

thiophenol

Downstream raw materials:

(R)-2-((phenylsulfonyl)methyl)butan-1-ol