C₆₅H₈₄N₄O₈

Base Information

Chemical Name:C₆₅H₈₄N₄O₈
CAS No.:1255150-27-6
Molecular Formula:C₆₅H₈₄N₄O₈
Molecular Weight:1049.4
Hs Code.:

C<sub>65</sub>H<sub>84</sub>N<sub>4</sub>O<sub>8</sub>

Synonyms:C₆₅H₈₄N₄O₈

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Chemical Property of C₆₅H₈₄N₄O₈

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Technology Process of C₆₅H₈₄N₄O₈

There total 7 articles about C₆₅H₈₄N₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1255150-26-5
C₇₇H₁₁₄N₄O₈Si₂

: 1255150-27-6
C₆₅H₈₄N₄O₈

Guidance literature:: C₇₇H₁₁₄N₄O₈Si₂; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 5h; Inert atmosphere;

With silver(l) oxide; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 155345-54-3
1-bromo-6-iodohexane

: 1255150-27-6
C₆₅H₈₄N₄O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / acetone / Reflux

2.1: sodium hydroxide / acetone / Reflux

3.1: tetrahydrofuran / 12 h / -78 - 20 °C

4.1: sodium t-butanolate; tri-tert-butyl phosphine / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / Reflux

5.1: ammonium acetate / acetic acid / 3 h / Reflux

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

6.2: 2 h / 20 °C / Inert atmosphere

With tri-tert-butyl phosphine; ammonium acetate; tetrabutyl ammonium fluoride; potassium carbonate; sodium hydroxide; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; acetic acid; acetone; toluene;

Reference yield:

: 1255150-22-1
C₂₁H₄₄BrNO₂Si

: 1255150-27-6
C₆₅H₈₄N₄O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / acetone / Reflux

2.1: tetrahydrofuran / 12 h / -78 - 20 °C

3.1: sodium t-butanolate; tri-tert-butyl phosphine / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / Reflux

4.1: ammonium acetate / acetic acid / 3 h / Reflux

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

5.2: 2 h / 20 °C / Inert atmosphere

With tri-tert-butyl phosphine; ammonium acetate; tetrabutyl ammonium fluoride; sodium hydroxide; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; acetic acid; acetone; toluene;