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(E)-2-(3-(4-bromophenyl)allyl)phenol

Base Information
  • Chemical Name:(E)-2-(3-(4-bromophenyl)allyl)phenol
  • CAS No.:201605-97-2
  • Molecular Formula:C15H13BrO
  • Molecular Weight:289.172
  • Hs Code.:
(E)-2-(3-(4-bromophenyl)allyl)phenol

Synonyms:(E)-2-(3-(4-bromophenyl)allyl)phenol

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Chemical Property of (E)-2-(3-(4-bromophenyl)allyl)phenol
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Technology Process of (E)-2-(3-(4-bromophenyl)allyl)phenol

There total 4 articles about (E)-2-(3-(4-bromophenyl)allyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
(2E)-3-(4-bromophenyl)-1-(2-hydroxyphenyl)prop-2-en-1-one; With chloroformic acid ethyl ester; In tetrahydrofuran; at 0 ℃; for 2h;
With sodium tetrahydroborate; In tetrahydrofuran; water; at 0 ℃; for 12h;
DOI:10.1021/jacs.8b02607
Guidance literature:
With aluminum oxide; In 1,2-dichloro-ethane; for 72h; Reflux;
Guidance literature:
Multi-step reaction with 2 steps
1.1: potassium hydroxide / methanol; water / 24 h / 20 °C / Inert atmosphere; Cooling with ice
2.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
2.2: 10 h / -5 °C / Inert atmosphere
With chloroformic acid ethyl ester; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; water; 1.1: |Aldol Condensation;
DOI:10.1021/ja510113s
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