N-phthaloyl-(S)-2-phenylglycyl chloride

Base Information

Chemical Name:N-phthaloyl-(S)-2-phenylglycyl chloride
CAS No.:1239896-95-7
Molecular Formula:C₁₆H₁₀ClNO₃
Molecular Weight:299.713
Hs Code.:

Synonyms:N-phthaloyl-(S)-2-phenylglycyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phthaloyl-(S)-2-phenylglycyl chloride

Chemical Property:

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Technology Process of N-phthaloyl-(S)-2-phenylglycyl chloride

There total 3 articles about N-phthaloyl-(S)-2-phenylglycyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 53178-27-1
2(S)-2-(1,3-dioxoisoindolin-2-yl)-2-phenylacetic acid

: 1239896-95-7
N-phthaloyl-(S)-2-phenylglycyl chloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In hexane; benzene; at 20 ℃;
DOI:10.1016/j.tetasy.2010.05.013

Reference yield:

: 85-44-9
phthalic anhydride

: 1239896-95-7
N-phthaloyl-(S)-2-phenylglycyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / Reflux; Schlenk technique; Inert atmosphere

2: thionyl chloride / toluene / Reflux; Schlenk technique; Inert atmosphere

With thionyl chloride; acetic acid; In toluene;
DOI:10.1055/s-0035-1560373

Reference yield:

: 2935-35-5
(S)-2-phenylglycine

: 1239896-95-7
N-phthaloyl-(S)-2-phenylglycyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / Reflux; Schlenk technique; Inert atmosphere

2: thionyl chloride / toluene / Reflux; Schlenk technique; Inert atmosphere

With thionyl chloride; acetic acid; In toluene;
DOI:10.1055/s-0035-1560373