N,N'-(1,2-phenylene)bis(1-(benzyloxy)-6-oxo-1,6-dihydropyridine-2-carboxamide)

Base Information

Chemical Name:N,N'-(1,2-phenylene)bis(1-(benzyloxy)-6-oxo-1,6-dihydropyridine-2-carboxamide)
CAS No.:1001404-13-2
Molecular Formula:C₃₂H₂₆N₄O₆
Molecular Weight:562.582
Hs Code.:

Synonyms:N,N'-(1,2-phenylene)bis(1-(benzyloxy)-6-oxo-1,6-dihydropyridine-2-carboxamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-(1,2-phenylene)bis(1-(benzyloxy)-6-oxo-1,6-dihydropyridine-2-carboxamide)

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Technology Process of N,N'-(1,2-phenylene)bis(1-(benzyloxy)-6-oxo-1,6-dihydropyridine-2-carboxamide)

There total 3 articles about N,N'-(1,2-phenylene)bis(1-(benzyloxy)-6-oxo-1,6-dihydropyridine-2-carboxamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 95-54-5
1,2-diamino-benzene

: 210366-17-9
1-(benzyloxy)-6-oxo-1,6-dihydropyridine-2-carboxylic acid chloride

: 1001404-13-2
N,N'-(1,2-phenylene)bis(1-(benzyloxy)-6-oxo-1,6-dihydropyridine-2-carboxamide)

Guidance literature:: With potassium carbonate; In dichloromethane; at 0 - 20 ℃; for 1h;

Reference yield:

: 210366-15-7
1-(benzyloxy)-2-oxo-1,2-dihydropyridine-6-carboxylic acid

: 1001404-13-2
N,N'-(1,2-phenylene)bis(1-(benzyloxy)-6-oxo-1,6-dihydropyridine-2-carboxamide)

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; N,N-dimethyl-formamide / 3 h / 78 °C / Inert atmosphere

2: potassium carbonate / dichloromethane; water / Inert atmosphere

With thionyl chloride; potassium carbonate; N,N-dimethyl-formamide; In dichloromethane; water;

Reference yield:

: 19621-92-2
2-oxo-1,2-dihydropyridine-6-carboxylic acid

: 1001404-13-2
N,N'-(1,2-phenylene)bis(1-(benzyloxy)-6-oxo-1,6-dihydropyridine-2-carboxamide)

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid; acetic acid; peracetic acid / 17 h / 80 °C / Inert atmosphere

2: potassium carbonate / methanol / 67 °C / Inert atmosphere

3: thionyl chloride; N,N-dimethyl-formamide / 3 h / 78 °C / Inert atmosphere

4: potassium carbonate / dichloromethane; water / Inert atmosphere

With peracetic acid; thionyl chloride; potassium carbonate; acetic acid; N,N-dimethyl-formamide; trifluoroacetic acid; In methanol; dichloromethane; water;