Allyl-4-cyclohexanon

Base Information

Chemical Name:Allyl-4-cyclohexanon
CAS No.:26845-57-8
Molecular Formula:C₉H₁₄O
Molecular Weight:138.21
Hs Code.:

Synonyms:Allyl-4-cyclohexanon

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Chemical Property of Allyl-4-cyclohexanon

Chemical Property:

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Technology Process of Allyl-4-cyclohexanon

There total 12 articles about Allyl-4-cyclohexanon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 20498-05-9
3-allylcyclohexanone

: 94-66-6
2-allylcyclohexan-1-one

: 26845-57-8
Allyl-4-cyclohexanon

Guidance literature:: 3-allylcyclohexanone; With trifluoromethylsulfonic anhydride; caesium carbonate; In 1,4-dioxane; toluene;

With dichloro(1,5-cyclooctadiene)palladium(II); 5-(trifluoromethyl)-2(1H)-pyridone; C₁₂H₂₃NO₄; C₁₁H₁₅NO; caesium carbonate; 2′-(diphenylphosphino)-N,N′-dimethyl-(1,1′-biphenyl)-2-amine; In toluene; at 100 ℃; for 24h;

With water; In toluene; Acidic conditions;
DOI:10.1126/science.abl7854

Reference yield: 10.0%

: 4-[3-(trimethylsilyl)prop-1-en-1-yl]cyclohexanone

: 26845-57-8
Allyl-4-cyclohexanon

: 7-vinylbicyclo[2.2.1]heptan-1-ol

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1246/bcsj.71.1639

Reference yield:

: 211995-75-4
4-methylene-1-(tetrahydropyran-2-yloxy)cyclohexane

: 26845-57-8
Allyl-4-cyclohexanon

Guidance literature:: Multi-step reaction with 6 steps

1.1: NaBH₄; 2-methylbut-2-ene; BF₃*OEt₂ / bis-(2-methoxy-ethyl) ether / 17 h / 20 °C

1.2: 90 percent / NaOH; H₂O₂ / bis-(2-methoxy-ethyl) ether; H₂O / 1.5 h / 0 - 40 °C

2.1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / -60 - 20 °C

3.1: 715.3 mg / tetrahydrofuran; hexane / 16 h / -60 - 20 °C

4.1: 77 percent / aq. HCl / tetrahydrofuran / 32 h / 20 °C

5.1: 82 percent / (COCl)2; DMSO; Et₃N / CH₂Cl₂ / -60 - 20 °C

6.1: BF₃*OEt₂ / CH₂Cl₂ / 1 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; 2-methyl-but-2-ene; oxalyl dichloride; boron trifluoride diethyl etherate; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; hexane; dichloromethane; diethylene glycol dimethyl ether; 1.1: Addition / 1.2: Oxidation / 2.1: Swern oxidation / 3.1: Wittig reaction / 4.1: Hydrolysis / 5.1: Swern oxidation / 6.1: Cyclization;
DOI:10.1246/bcsj.71.1639