2-((2,6-dimethyl-4-sulfonatophenylimino)methyl)pyridine sodium

Base Information

Chemical Name:2-((2,6-dimethyl-4-sulfonatophenylimino)methyl)pyridine sodium
CAS No.:613230-30-1
Molecular Formula:C₁₄H₁₃N₂O₃S*Na
Molecular Weight:312.325
Hs Code.:

Synonyms:2-((2,6-dimethyl-4-sulfonatophenylimino)methyl)pyridine sodium

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Chemical Property of 2-((2,6-dimethyl-4-sulfonatophenylimino)methyl)pyridine sodium

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Technology Process of 2-((2,6-dimethyl-4-sulfonatophenylimino)methyl)pyridine sodium

There total 1 articles about 2-((2,6-dimethyl-4-sulfonatophenylimino)methyl)pyridine sodium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 613230-30-1
2-((2,6-dimethyl-4-sulfonatophenylimino)methyl)pyridine sodium

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; sodium hydroxide / 180 - 190 °C

2: toluene

With sulfuric acid; sodium hydroxide; In toluene;
DOI:10.1007/s11243-011-9564-1

Reference yield: 80.0%

: [iridium(III)(μ-chloro)(2-phenylpyridine)2]2

: 613230-30-1
2-((2,6-dimethyl-4-sulfonatophenylimino)methyl)pyridine sodium

: C₃₆H₂₉IrN₄O₃S

Guidance literature:: In methanol; chloroform; at 20 ℃; for 24h;
DOI:10.1016/j.dyepig.2020.108220

Reference yield: 76.0%

: 17457-51-1,17836-09-8,55449-91-7
dichlorobis(dimethylsulfide)platinum(II)

: 613230-30-1
2-((2,6-dimethyl-4-sulfonatophenylimino)methyl)pyridine sodium

: 613230-34-5
sodium 2-((2,6-dimethyl-4-sulfonatophenylimino)methyl)pyridine platinum(II) dichloride

Guidance literature:: In dimethyl sulfoxide; Schlenk flask; soln. of ligand was added to the Pt complex, mixt. was stirred overnight; CH2Cl2 was added, ppt. was filtered off, washed with DCM, dissolved in MeOH, pptd. with Et2O, dried under vac.; elem. anal.;
DOI:10.1016/S0022-328X(03)00540-0