4-benzyl-6-trifluoromethyl-5,6-dihydro-3-methyl-4H-1,2,4-oxadiazin-6-ol

Base Information

Chemical Name:4-benzyl-6-trifluoromethyl-5,6-dihydro-3-methyl-4H-1,2,4-oxadiazin-6-ol
CAS No.:1426231-11-9
Molecular Formula:C₁₂H₁₃F₃N₂O₂
Molecular Weight:274.243
Hs Code.:

Synonyms:4-benzyl-6-trifluoromethyl-5,6-dihydro-3-methyl-4H-1,2,4-oxadiazin-6-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-benzyl-6-trifluoromethyl-5,6-dihydro-3-methyl-4H-1,2,4-oxadiazin-6-ol

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Technology Process of 4-benzyl-6-trifluoromethyl-5,6-dihydro-3-methyl-4H-1,2,4-oxadiazin-6-ol

There total 2 articles about 4-benzyl-6-trifluoromethyl-5,6-dihydro-3-methyl-4H-1,2,4-oxadiazin-6-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 220354-32-5
3-benzyl-4-trifluoroacetyl-2-methyl-1,3-oxazol-3-ium-5-olate

: 1426231-11-9
4-benzyl-6-trifluoromethyl-5,6-dihydro-3-methyl-4H-1,2,4-oxadiazin-6-ol

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In N,N-dimethyl-formamide; at 0 - 80 ℃; for 4h; regiospecific reaction; Inert atmosphere;
DOI:10.3987/COM-12-12627

Reference yield:

: 7662-79-5
2-(N-benzylacetamido)acetic acid

: 1426231-11-9
4-benzyl-6-trifluoromethyl-5,6-dihydro-3-methyl-4H-1,2,4-oxadiazin-6-ol

Guidance literature:: Multi-step reaction with 2 steps

1: ethyl acetate / 3 h / 0 - 20 °C

2: hydroxylamine hydrochloride; sodium acetate / N,N-dimethyl-formamide / 4 h / 0 - 80 °C / Inert atmosphere

With hydroxylamine hydrochloride; sodium acetate; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.3987/COM-12-12627