2,6-di(tert-butyl)-4-(5-sulfanyl-1,3,4-thiadiazol-2-yl)benzenol

Base Information

• Chemical Name: 2,6-di(tert-butyl)-4-(5-sulfanyl-1,3,4-thiadiazol-2-yl)benzenol
• CAS No.: 130116-03-9
• Molecular Formula: C₁₆H₂₂N₂OS₂
• Molecular Weight: 322.495
• Mol file: 130116-03-9.mol

Synonyms:Cl-986

Chemical Property of 2,6-di(tert-butyl)-4-(5-sulfanyl-1,3,4-thiadiazol-2-yl)benzenol

Chemical Property:

Purity/Quality:

2,6-Di(tert-butyl)-4-(5-sulfanyl-1,3,4-thiadiazol-2-yl)benzenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,6-di(tert-butyl)-4-(5-sulfanyl-1,3,4-thiadiazol-2-yl)benzenol

There total 11 articles about 2,6-di(tert-butyl)-4-(5-sulfanyl-1,3,4-thiadiazol-2-yl)benzenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

5-<3,5-bis(1,1-dimethylethyl)-4-methoxyphenyl>-1,3,4-thiazole-2(3H)-thione (148773-28-8) → Cl-986 (130116-03-9)

Guidance literature:

With sodium thiomethoxide; In N,N-dimethyl-formamide; at 120 ℃; for 3h;

DOI:10.1021/jm00060a017

Reference yield: 76.0%

carbon disulfide (75-15-0,12122-00-8) + 3,5-bis(1,1-dimethylethyl)-4-hydroxybenzenecarbothionic acid, hydrazide (3202-96-8) → Cl-986 (130116-03-9)

Guidance literature:

In ethanol; for 2h; Heating;

DOI:10.1021/jm00060a017

Reference yield: 69.0%

carbon disulfide (75-15-0,12122-00-8) + 3,5-bis(1,1-dimethylethyl)-N,4-dihydroxybenzenecarboximidic acid hydrazide (130116-80-2) → Cl-986 (130116-03-9)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1021/jm00060a017

upstream raw materials:

carbon disulfide

3,5-bis(1,1-dimethylethyl)-4-hydroxybenzenecarbothionic acid, hydrazide

3,5-bis(1,1-dimethylethyl)-N,4-dihydroxybenzenecarboximidic acid hydrazide

5-<3,5-bis(1,1-dimethylethyl)-4-methoxyphenyl>-1,3,4-thiazole-2(3H)-thione

Downstream raw materials:

2,6-Di-tert-butyl-4-(5-methylsulfanyl-[1,3,4]thiadiazol-2-yl)-phenol

Refernces