N-[(1R,2aS,4aS,5S,5aR,12bR)-5-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-1,2a,4a,5,5a,12b-hexahydro-phenanthro[2,3-d][1,3]dioxol-1-yl]-4-methyl-benzenesulfonamide

Base Information

Chemical Name:N-[(1R,2aS,4aS,5S,5aR,12bR)-5-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-1,2a,4a,5,5a,12b-hexahydro-phenanthro[2,3-d][1,3]dioxol-1-yl]-4-methyl-benzenesulfonamide
CAS No.:1006585-86-9
Molecular Formula:C₃₁H₄₁NO₇SSi
Molecular Weight:599.821
Hs Code.:

N-[(1R,2aS,4aS,5S,5aR,12bR)-5-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-1,2a,4a,5,5a,12b-hexahydro-phenanthro[2,3-d][1,3]dioxol-1-yl]-4-methyl-benzenesulfonamide

Synonyms:N-[(1R,2aS,4aS,5S,5aR,12bR)-5-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-1,2a,4a,5,5a,12b-hexahydro-phenanthro[2,3-d][1,3]dioxol-1-yl]-4-methyl-benzenesulfonamide

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Chemical Property of N-[(1R,2aS,4aS,5S,5aR,12bR)-5-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-1,2a,4a,5,5a,12b-hexahydro-phenanthro[2,3-d][1,3]dioxol-1-yl]-4-methyl-benzenesulfonamide

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Technology Process of N-[(1R,2aS,4aS,5S,5aR,12bR)-5-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-1,2a,4a,5,5a,12b-hexahydro-phenanthro[2,3-d][1,3]dioxol-1-yl]-4-methyl-benzenesulfonamide

There total 1 articles about N-[(1R,2aS,4aS,5S,5aR,12bR)-5-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-1,2a,4a,5,5a,12b-hexahydro-phenanthro[2,3-d][1,3]dioxol-1-yl]-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1006585-85-8
C₃₁H₄₁NO₇SSi

: 1006585-86-9
N-[(1R,2aS,4aS,5S,5aR,12bR)-5-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-1,2a,4a,5,5a,12b-hexahydro-phenanthro[2,3-d][1,3]dioxol-1-yl]-4-methyl-benzenesulfonamide

Guidance literature:: With silica gel; at 120 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jo1003136

Reference yield: 89.0%

: 1006585-86-9
N-[(1R,2aS,4aS,5S,5aR,12bR)-5-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-1,2a,4a,5,5a,12b-hexahydro-phenanthro[2,3-d][1,3]dioxol-1-yl]-4-methyl-benzenesulfonamide

: 1006585-88-1
N-[(1R,2aS,4aS,5S,5aS,12bR)-5-(tert-butyl-dimethyl-silanyloxy)-6-hydroxy-3,3-dimethyl-7-oxo-1,2a,4a,5,5a,6,7,12b-octahydro-phenanthro[2,3-d][1,3]dioxol-1-yl]-4-methyl-benzenesulfonamide

Guidance literature:: N-[(1R,2aS,4aS,5S,5aR,12bR)-5-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-1,2a,4a,5,5a,12b-hexahydro-phenanthro[2,3-d][1,3]dioxol-1-yl]-4-methyl-benzenesulfonamide; With 4-methylmorpholine N-oxide; In dichloromethane; for 0.166667h;

With osmium(VIII) oxide; water; In dichloromethane; for 10h;

Reference yield: 89.0%

: 1006585-86-9
N-[(1R,2aS,4aS,5S,5aR,12bR)-5-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-1,2a,4a,5,5a,12b-hexahydro-phenanthro[2,3-d][1,3]dioxol-1-yl]-4-methyl-benzenesulfonamide

: 1224711-82-3
C₃₁H₄₁NO₉SSi

Guidance literature:: With osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 10h; Inert atmosphere;
DOI:10.1021/jo1003136