C₆₅H₁₀₃O₁₅N₅SiO

Base Information

Chemical Name:C₆₅H₁₀₃O₁₅N₅SiO
CAS No.:220440-10-8
Molecular Formula:C₆₅H₁₀₃N₅O₁₆Si
Molecular Weight:1238.64
Hs Code.:

C<sub>65</sub>H<sub>103</sub>O<sub>15</sub>N<sub>5</sub>SiO

Synonyms:C₆₅H₁₀₃O₁₅N₅SiO

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Chemical Property of C₆₅H₁₀₃O₁₅N₅SiO

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Technology Process of C₆₅H₁₀₃O₁₅N₅SiO

There total 11 articles about C₆₅H₁₀₃O₁₅N₅SiO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: C₆₅H₁₀₃N₅O₁₅Si

: 220440-10-8
C₆₅H₁₀₃O₁₅N₅SiO

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 20 ℃; Further Variations:; Reagents; Solvents; Product distribution;
DOI:10.1021/jo0105991

Reference yield:

: 74163-81-8
L-Tic-OH

: 220440-10-8
C₆₅H₁₀₃O₁₅N₅SiO

Guidance literature:: Multi-step reaction with 9 steps

1.1: 97 percent / NaHCO₃ / H₂O / 1.5 h / 20 °C

2.1: 89 percent / Et₃N; DMAP; isopropenyl chloroformate / CH₂Cl₂ / 1 h / 0 °C

3.1: 86 percent / H₂ / Pd/C / methanol; ethyl acetate / 3 h / 2068.65 Torr

4.1: BOP-Cl; NMM / CH₂Cl₂ / 0.5 h / -15 °C

4.2: 60 percent / NMM / CH₂Cl₂ / 6 h / 0 °C

5.1: 100 percent / MgBr₂*Et₂O / CH₂Cl₂ / 4.5 h / -20 - 0 °C

6.1: 47 percent / NMM; isopropenyl chloroformate / CH₂Cl₂ / 4 h / -15 - 20 °C

7.1: 83 percent / aq. AcOH / tetrahydrofuran / 16 h

8.1: Dess-Martin periodinane / CH₂Cl₂ / 2 h

9.1: 100 percent / 2-methyl-2-butene; NaH₂PO₄; NaClO₂ / 2-methyl-propan-2-ol; H₂O / 20 °C

With 4-methyl-morpholine; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; Isopropenyl chloroformate; hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; triethylamine; magnesium bromide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol; 8.1: Dess-Martin oxidation;
DOI:10.1021/jo0105991

Reference yield:

: 79261-58-8
(S)-3,4-dihydro-1H-isoquinoline-2,3-dicarboxylic acid 2-benzyl ester

: 220440-10-8
C₆₅H₁₀₃O₁₅N₅SiO

Guidance literature:: Multi-step reaction with 8 steps

1.1: 89 percent / Et₃N; DMAP; isopropenyl chloroformate / CH₂Cl₂ / 1 h / 0 °C

2.1: 86 percent / H₂ / Pd/C / methanol; ethyl acetate / 3 h / 2068.65 Torr

3.1: BOP-Cl; NMM / CH₂Cl₂ / 0.5 h / -15 °C

3.2: 60 percent / NMM / CH₂Cl₂ / 6 h / 0 °C

4.1: 100 percent / MgBr₂*Et₂O / CH₂Cl₂ / 4.5 h / -20 - 0 °C

5.1: 47 percent / NMM; isopropenyl chloroformate / CH₂Cl₂ / 4 h / -15 - 20 °C

6.1: 83 percent / aq. AcOH / tetrahydrofuran / 16 h

7.1: Dess-Martin periodinane / CH₂Cl₂ / 2 h

8.1: 100 percent / 2-methyl-2-butene; NaH₂PO₄; NaClO₂ / 2-methyl-propan-2-ol; H₂O / 20 °C

With 4-methyl-morpholine; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; Isopropenyl chloroformate; hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; Dess-Martin periodane; acetic acid; triethylamine; magnesium bromide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol; 7.1: Dess-Martin oxidation;
DOI:10.1021/jo0105991