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Technology Process of (C6H13)3Si(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)C6H4(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)Si(C6H13)3

(C6H13)3Si(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)C6H4(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)Si(C6H13)3

Base Information
  • Chemical Name:(C6H13)3Si(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)C6H4(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)Si(C6H13)3
  • CAS No.:207971-17-3
  • Molecular Formula:C146H182N8Si2Zn2
  • Molecular Weight:2236.06
  • Hs Code.:
(C<sub>6</sub>H<sub>13</sub>)3Si(CCZn(CC<sub>4</sub>H<sub>2</sub>NC(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)C<sub>4</sub>H<sub>2</sub>N)2CC)C<sub>6</sub>H<sub>4</sub>(CCZn(CC<sub>4</sub>H<sub>2</sub>NC(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)C<sub>4</sub>H<sub>2</sub>N)2CC)Si(C<sub>6</sub>H<sub>13</sub>)3

Synonyms:(C6H13)3Si(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)C6H4(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)Si(C6H13)3

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Chemical Property of (C6H13)3Si(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)C6H4(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)Si(C6H13)3
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Technology Process of (C6H13)3Si(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)C6H4(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)Si(C6H13)3

There total 1 articles about (C6H13)3Si(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)C6H4(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)Si(C6H13)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

(C<sub>6</sub>H<sub>13</sub>)3Si(C<sub>2</sub>C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>Zn(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)2C<sub>2</sub>)H
207971-15-1

(C6H13)3Si(C2C20H8N4Zn(C6H3(C(CH3)3)2)2C2)H

para-diiodobenzene
624-38-4,1032416-46-8

para-diiodobenzene

(C<sub>6</sub>H<sub>13</sub>)3Si(CCZn(CC<sub>4</sub>H<sub>2</sub>NC(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)C<sub>4</sub>H<sub>2</sub>N)2CC)C<sub>6</sub>H<sub>4</sub>(CCZn(CC<sub>4</sub>H<sub>2</sub>NC(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)C<sub>4</sub>H<sub>2</sub>N)2CC)Si(C<sub>6</sub>H<sub>13</sub>)3
207971-17-3

(C6H13)3Si(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)C6H4(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)Si(C6H13)3

Guidance literature:
With Me2NSnMe3; PPh3; tris(dibenzylideneacetone)dipalladium (0); In not given; addn. of Me2NSnMe3 to the Zn complex, addn. of the diiodide in the presence of Pd2(dba)3 and PPh3;
DOI:10.1002/(SICI)1521-3773(19980420)37:7<986::AID-ANIE986>3.0.CO;2-D

Reference yield:

1,4-diaza-bicyclo[2.2.2]octane
280-57-9,88935-43-7

1,4-diaza-bicyclo[2.2.2]octane

(C<sub>6</sub>H<sub>13</sub>)3Si(CCZn(CC<sub>4</sub>H<sub>2</sub>NC(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)C<sub>4</sub>H<sub>2</sub>N)2CC)C<sub>6</sub>H<sub>4</sub>(CCZn(CC<sub>4</sub>H<sub>2</sub>NC(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)C<sub>4</sub>H<sub>2</sub>N)2CC)Si(C<sub>6</sub>H<sub>13</sub>)3
207971-17-3

(C6H13)3Si(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)C6H4(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)Si(C6H13)3

4Zn<sup>(2+)</sup>*2C<sub>146</sub>H<sub>182</sub>N<sub>8</sub>Si<sub>2</sub><sup>(4-)</sup>*2C<sub>6</sub>H<sub>12</sub>N<sub>2</sub>=((C<sub>6</sub>H<sub>13</sub>)3Si(CCZn(CC<sub>4</sub>H<sub>2</sub>NC(C<sub>6</sub>H<sub>3</sub>(C(CH<sub>3</sub>)3)2)C<sub>4</sub>H<sub>2</sub>N)2CC)2C<sub>6</sub>H<sub>4</sub>Si(C<sub>6</sub>H<sub>13</sub>)3)2(C<sub>6</sub>H<sub>12</sub>N<sub>2</sub>)2

4Zn(2+)*2C146H182N8Si2(4-)*2C6H12N2=((C6H13)3Si(CCZn(CC4H2NC(C6H3(C(CH3)3)2)C4H2N)2CC)2C6H4Si(C6H13)3)2(C6H12N2)2

Guidance literature:
In not given; followed by (1)H NMR;
DOI:10.1021/ja992821d
upstream raw materials:

(C6H13)3Si(C2C20H8N4Zn(C6H3(C(CH3)3)2)2C2)H

para-diiodobenzene

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