10-chloro-N-cyclohexyl-5-oxo-6-propyl-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide

Base Information

Chemical Name:10-chloro-N-cyclohexyl-5-oxo-6-propyl-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide
CAS No.:1427311-23-6
Molecular Formula:C₂₆H₂₈ClN₃O₂
Molecular Weight:449.98
Hs Code.:

Synonyms:10-chloro-N-cyclohexyl-5-oxo-6-propyl-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide

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Chemical Property of 10-chloro-N-cyclohexyl-5-oxo-6-propyl-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide

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Technology Process of 10-chloro-N-cyclohexyl-5-oxo-6-propyl-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide

There total 6 articles about 10-chloro-N-cyclohexyl-5-oxo-6-propyl-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1427311-39-4
C₂₆H₂₉ClIN₃O₂

: 1427311-23-6
10-chloro-N-cyclohexyl-5-oxo-6-propyl-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide

Guidance literature:: With copper(l) iodide; potassium carbonate; L-proline; In dimethyl sulfoxide; at 90 ℃; for 0.666667h; Microwave irradiation; Inert atmosphere;
DOI:10.1039/c3cc00111c

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 1427311-23-6
10-chloro-N-cyclohexyl-5-oxo-6-propyl-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol / 0.17 h / 20 °C / Inert atmosphere

1.2: 0.08 h / Inert atmosphere

1.3: 72 h / 20 °C / Inert atmosphere

2.1: copper(l) iodide; L-proline; potassium carbonate / dimethyl sulfoxide / 0.67 h / 90 °C / Microwave irradiation; Inert atmosphere

With copper(l) iodide; potassium carbonate; L-proline; In methanol; dimethyl sulfoxide;
DOI:10.1039/c3cc00111c

Reference yield:

: 931-53-3
Cyclohexyl isocyanide

: 1427311-23-6
10-chloro-N-cyclohexyl-5-oxo-6-propyl-6,7-dihydro-5H-benzo[6,7][1,4]diazepino[1,2-a]indole-7-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol / 0.17 h / 20 °C / Inert atmosphere

1.2: 0.08 h / Inert atmosphere

1.3: 72 h / 20 °C / Inert atmosphere

2.1: copper(l) iodide; L-proline; potassium carbonate / dimethyl sulfoxide / 0.67 h / 90 °C / Microwave irradiation; Inert atmosphere

With copper(l) iodide; potassium carbonate; L-proline; In methanol; dimethyl sulfoxide;
DOI:10.1039/c3cc00111c