2-(2,2'-bipyridin-5-ylethynyl)-4-tert-butylphenyl trifluoromethanesulfonate

Base Information

Chemical Name:2-(2,2'-bipyridin-5-ylethynyl)-4-tert-butylphenyl trifluoromethanesulfonate
CAS No.:1099699-38-3
Molecular Formula:C₂₃H₁₉F₃N₂O₃S
Molecular Weight:460.477
Hs Code.:

Synonyms:2-(2,2'-bipyridin-5-ylethynyl)-4-tert-butylphenyl trifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2,2'-bipyridin-5-ylethynyl)-4-tert-butylphenyl trifluoromethanesulfonate

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Technology Process of 2-(2,2'-bipyridin-5-ylethynyl)-4-tert-butylphenyl trifluoromethanesulfonate

There total 1 articles about 2-(2,2'-bipyridin-5-ylethynyl)-4-tert-butylphenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 217966-72-8
4-(tert-butyl)-2-iodophenyltrifluoromethane sulfonate

: 162318-34-5
5-ethynyl-2,2'-bipyridine

: 1099699-38-3
2-(2,2'-bipyridin-5-ylethynyl)-4-tert-butylphenyl trifluoromethanesulfonate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1039/b812261j

Reference yield: 95.0%

: 1099699-38-3
2-(2,2'-bipyridin-5-ylethynyl)-4-tert-butylphenyl trifluoromethanesulfonate

: 115-19-5
2-methyl-but-3-yn-2-ol

: 1099699-39-4
4-[2-(2,2'-bipyridin-5-ylethynyl)-4-tert-butylphenyl]-2-methylbut-3-yn-2-ol

Guidance literature:: With copper(l) iodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; diisopropylamine; In N,N-dimethyl-formamide; at 80 ℃; for 14h; Inert atmosphere;
DOI:10.1039/b812261j