Bicyclo[4.4.1]undeca-1(10),2,4,6,8-pentaene-2-carbonyl chloride

Base Information

Chemical Name:Bicyclo[4.4.1]undeca-1(10),2,4,6,8-pentaene-2-carbonyl chloride
CAS No.:106817-62-3
Molecular Formula:C₁₂H₉ClO
Molecular Weight:204.656
Hs Code.:2916209090
DSSTox Substance ID:DTXSID40545248
Mol file:106817-62-3.mol

Synonyms:106817-62-3;Bicyclo[4.4.1]undeca-1(10),2,4,6,8-pentaene-2-carbonyl chloride;Bicyclo[4.4.1]undeca-1,3,5,7,9-pentaene-2-carbonyl chloride (9CI);DTXSID40545248

Suppliers and Price of Bicyclo[4.4.1]undeca-1(10),2,4,6,8-pentaene-2-carbonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Bicyclo[4.4.1]undeca-1(10),2,4,6,8-pentaene-2-carbonyl chloride

Chemical Property:

PSA：17.07000
LogP:3.09420
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:204.0341926
Heavy Atom Count:14
Complexity:214

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2=CC=CC=C1C(=CC=C2)C(=O)Cl

Technology Process of Bicyclo[4.4.1]undeca-1(10),2,4,6,8-pentaene-2-carbonyl chloride

There total 1 articles about Bicyclo[4.4.1]undeca-1(10),2,4,6,8-pentaene-2-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5873-56-3,34029-50-0,34029-51-1
1,6-Methano-<10>annulen-2-carbonsaeure

: 106817-62-3
Bicyclo<4.4.1>undeca-1,3,5,7,9-pentaen-2-carbonsaeure-chlorid

Guidance literature:: With thionyl chloride;

Reference yield:

: 106817-62-3
Bicyclo<4.4.1>undeca-1,3,5,7,9-pentaen-2-carbonsaeure-chlorid

: 10-Benzoyl-N,N-diethylbicyclo<4.4.1>undeca-1,3,5,7,9-pentaen-2-carbonsaeureamid

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / diethyl ether / 1 h / Ambient temperature

2: 2.5 M BuLi, TMEDA / tetrahydrofuran; hexane / 1 h / -78 °C

3: 47.5 percent / tetrahydrofuran / 16 h / Ambient temperature

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1002/hlca.19860690531

Reference yield:

: 106817-62-3
Bicyclo<4.4.1>undeca-1,3,5,7,9-pentaen-2-carbonsaeure-chlorid

: 6074-92-6
Bicyclo<4.4.1>undeca-1,3,5,7,9-pentaen-2,10-dicarbonsaeure-anhydrid

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / diethyl ether / 1 h / Ambient temperature

2: 2.5 M BuLi, TMEDA / tetrahydrofuran; hexane / 1 h / -78 °C

3: tetrahydrofuran / 0.25 h / -78 °C

4: acetonitrile / 1 h / Heating

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; diethyl ether; hexane; acetonitrile;
DOI:10.1002/hlca.19860690531