2-(3,4-dimethoxy-α-hydroxybenzyl)-4,5-methylenedioxybenzaldehyde dimethylacetal

Base Information

Chemical Name:2-(3,4-dimethoxy-α-hydroxybenzyl)-4,5-methylenedioxybenzaldehyde dimethylacetal
CAS No.:74879-24-6
Molecular Formula:C₁₉H₂₂O₇
Molecular Weight:362.379
Hs Code.:

Synonyms:2-(3,4-dimethoxy-α-hydroxybenzyl)-4,5-methylenedioxybenzaldehyde dimethylacetal

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Chemical Property of 2-(3,4-dimethoxy-α-hydroxybenzyl)-4,5-methylenedioxybenzaldehyde dimethylacetal

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Technology Process of 2-(3,4-dimethoxy-α-hydroxybenzyl)-4,5-methylenedioxybenzaldehyde dimethylacetal

There total 3 articles about 2-(3,4-dimethoxy-α-hydroxybenzyl)-4,5-methylenedioxybenzaldehyde dimethylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 74879-22-4
6-bromobenzo-1,3-dioxole-5-carboxaldehyde dimethyl acetal

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 74879-24-6
2-(3,4-dimethoxy-α-hydroxybenzyl)-4,5-methylenedioxybenzaldehyde dimethylacetal

Guidance literature:: With n-butyllithium; In diethyl ether; for 0.5h;

Reference yield: 76.0%

: 74879-24-6
2-(3,4-dimethoxy-α-hydroxybenzyl)-4,5-methylenedioxybenzaldehyde dimethylacetal

Guidance literature:

Reference yield:

: 15930-53-7
6-bromo-3,4-methylenedioxybenzaldehyde

: 74879-24-6
2-(3,4-dimethoxy-α-hydroxybenzyl)-4,5-methylenedioxybenzaldehyde dimethylacetal

Guidance literature:: Multi-step reaction with 2 steps

1: Dowex 50W-X₈ acid exchange resin / methanol / 20 h / Heating

2: 91 percent / 1.) n-BuLi / diethyl ether / 0.5 h

With n-butyllithium; Dowex 50W-X₈ acid exchange resin; In methanol; diethyl ether;