Technology Process of Z(OMe)-Asn-Ser-Ile-Leu-Asn-NH2
There total 9 articles about Z(OMe)-Asn-Ser-Ile-Leu-Asn-NH2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; dimethyl sulfoxide;
at 4 ℃;
for 40h;
DOI:10.1248/cpb.28.1873
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1) Et3N, 2) DCC / 2) DMF, THF, 24 h
2: 80percent hydrazine hydrate / methanol
3: diazotizing reagent
4: 90 percent / Et3N / dimethylsulfoxide; hexamethylphosphoric acid triamide / 40 h / 4 °C
5: 90 percent / Et3N / dimethylsulfoxide; hexamethylphosphoric acid triamide / 40 h / 4 °C
With
diazotizing reagent; hydrazine hydrate; triethylamine; dicyclohexyl-carbodiimide;
In
methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dimethyl sulfoxide;
DOI:10.1248/cpb.28.1873
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1) Et3N, 2) DCC / 2) DMF, THF, 24 h
2: 80percent hydrazine hydrate / methanol
3: diazotizing reagent
4: 90 percent / Et3N / dimethylsulfoxide; hexamethylphosphoric acid triamide / 40 h / 4 °C
5: 90 percent / Et3N / dimethylsulfoxide; hexamethylphosphoric acid triamide / 40 h / 4 °C
With
diazotizing reagent; hydrazine hydrate; triethylamine; dicyclohexyl-carbodiimide;
In
methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dimethyl sulfoxide;
DOI:10.1248/cpb.28.1873
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