{2-[3-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-5-methyl-phenyl]-1-chlorocarbonyl-ethyl}-methyl-carbamic acid 9H-fluoren-9-ylmethyl ester

Base Information

• Chemical Name: {2-[3-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-5-methyl-phenyl]-1-chlorocarbonyl-ethyl}-methyl-carbamic acid 9H-fluoren-9-ylmethyl ester
• CAS No.: 557785-60-1
• Molecular Formula: C₃₃H₄₀ClNO₅Si
• Molecular Weight: 594.223

Synonyms:{2-[3-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-5-methyl-phenyl]-1-chlorocarbonyl-ethyl}-methyl-carbamic acid 9H-fluoren-9-ylmethyl ester

Chemical Property of {2-[3-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-5-methyl-phenyl]-1-chlorocarbonyl-ethyl}-methyl-carbamic acid 9H-fluoren-9-ylmethyl ester

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Technology Process of {2-[3-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-5-methyl-phenyl]-1-chlorocarbonyl-ethyl}-methyl-carbamic acid 9H-fluoren-9-ylmethyl ester

There total 1 articles about {2-[3-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-5-methyl-phenyl]-1-chlorocarbonyl-ethyl}-methyl-carbamic acid 9H-fluoren-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-[3-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-5-methyl-phenyl]-2-[(9H-fluoren-9-ylmethoxycarbonyl)-methyl-amino]-propionic acid (575444-10-9) → {2-[3-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-5-methyl-phenyl]-1-chlorocarbonyl-ethyl}-methyl-carbamic acid 9H-fluoren-9-ylmethyl ester (557785-60-1)

Guidance literature:

With oxalyl dichloride;

DOI:10.1021/ol034575n

Reference yield: 84.0%

{2-[3-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-5-methyl-phenyl]-1-chlorocarbonyl-ethyl}-methyl-carbamic acid 9H-fluoren-9-ylmethyl ester (557785-60-1) + 1-benzyl-5-benzyloxy-4-benzyloxymethyl-6,8-dimethoxy-7-methyl-2a,3,4,8b-tetrahydro-1H-1,3-diaza-cyclobuta[a]naphthalen-2-one (557785-59-8) → C68H75N3O10Si (557785-61-2)

Guidance literature:

With dmap; In dichloromethane;

DOI:10.1021/ol034575n

Reference yield:

(1R,3S)-8-Allyloxy-1-allyloxymethyl-3-(tert-butyl-dimethyl-silanyloxymethyl)-5,7-dimethoxy-6-methyl-1,2,3,4-tetrahydro-isoquinoline (866110-67-0) + {2-[3-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-5-methyl-phenyl]-1-chlorocarbonyl-ethyl}-methyl-carbamic acid 9H-fluoren-9-ylmethyl ester (557785-60-1) → C59H82N2O10Si2 (942197-84-4)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 2h;

DOI:10.1016/j.tetlet.2007.03.113

upstream raw materials:

3-[3-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-5-methyl-phenyl]-2-[(9H-fluoren-9-ylmethoxycarbonyl)-methyl-amino]-propionic acid

Downstream raw materials:

C₆₈H₇₅N₃O₁₀Si

C₅₉H₈₂N₂O₁₀Si₂

C₅₃H₆₈N₂O₁₀Si

C₅₃H₆₆N₂O₁₀Si

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