2,5-Dimethoxy-3,6-bis-[12-(tetrahydro-pyran-2-yloxy)-dodecyl]-benzene-1,4-diamine

Base Information

Chemical Name:2,5-Dimethoxy-3,6-bis-[12-(tetrahydro-pyran-2-yloxy)-dodecyl]-benzene-1,4-diamine
CAS No.:343862-95-3
Molecular Formula:C₄₂H₇₆N₂O₆
Molecular Weight:705.075
Hs Code.:

Synonyms:2,5-Dimethoxy-3,6-bis-[12-(tetrahydro-pyran-2-yloxy)-dodecyl]-benzene-1,4-diamine

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Chemical Property of 2,5-Dimethoxy-3,6-bis-[12-(tetrahydro-pyran-2-yloxy)-dodecyl]-benzene-1,4-diamine

Chemical Property:

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Technology Process of 2,5-Dimethoxy-3,6-bis-[12-(tetrahydro-pyran-2-yloxy)-dodecyl]-benzene-1,4-diamine

There total 11 articles about 2,5-Dimethoxy-3,6-bis-[12-(tetrahydro-pyran-2-yloxy)-dodecyl]-benzene-1,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77798-75-5
2,5-Dinitro-3,6-bis<12-(tetrahydro-2-pyranyloxy)dodecyl>hydrochinon-dimethylether

: 343862-95-3
2,5-Dimethoxy-3,6-bis-[12-(tetrahydro-pyran-2-yloxy)-dodecyl]-benzene-1,4-diamine

Guidance literature:: With hydrogen; nickel; In benzene; at 80 ℃; for 5h; under 73550.8 Torr;

Reference yield:

: 1108-58-3
<10-(Methoxycarbonyl)decyl>triphenylphosphoniumiodid

: 343862-95-3
2,5-Dimethoxy-3,6-bis-[12-(tetrahydro-pyran-2-yloxy)-dodecyl]-benzene-1,4-diamine

Guidance literature:: Multi-step reaction with 11 steps

1: NaOMe / dimethylformamide / 1) 0 deg C, 10 min, 2) r.t., 1.5 h

2: 70 percent / dimethylformamide / 3 h / Ambient temperature

3: 90 percent / H₂ / Raney-Ni / methanol / 5 h / 70 °C / 44130.5 Torr

4: 48percent HBr / acetic acid / 14 h / 110 °C

5: pyridine / 14 h / Ambient temperature

6: 69 percent / conc. HNO₃ / propionic acid / 240 h / Ambient temperature

7: 8.2 g / H₂SO₃, SO₂ / acetic acid / 5 h / 80 °C

8: 58 percent / K₂CO₃ / acetone / 4 h / Heating

9: 84 percent / CaCl₂, NaBH₄ / tetrahydrofuran / 48 h / Ambient temperature

10: 86 percent / HCl / diethyl ether / 24 h / Ambient temperature

11: H₂ / Raney-Ni / benzene / 5 h / 80 °C / 73550.8 Torr

With hydrogenchloride; sodium tetrahydroborate; sulfur dioxide; hydrogen bromide; hydrogen; nitric acid; sodium methylate; sulphurous acid; potassium carbonate; calcium chloride; nickel; In tetrahydrofuran; pyridine; methanol; diethyl ether; acetic acid; propionic acid; N,N-dimethyl-formamide; acetone; benzene;

Reference yield:

: 343859-17-6
12-[4-(11-Carboxy-undecyl)-2,5-dihydroxy-phenyl]-dodecanoic acid

: 343862-95-3
2,5-Dimethoxy-3,6-bis-[12-(tetrahydro-pyran-2-yloxy)-dodecyl]-benzene-1,4-diamine

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine / 14 h / Ambient temperature

2: 69 percent / conc. HNO₃ / propionic acid / 240 h / Ambient temperature

3: 8.2 g / H₂SO₃, SO₂ / acetic acid / 5 h / 80 °C

4: 58 percent / K₂CO₃ / acetone / 4 h / Heating

5: 84 percent / CaCl₂, NaBH₄ / tetrahydrofuran / 48 h / Ambient temperature

6: 86 percent / HCl / diethyl ether / 24 h / Ambient temperature

7: H₂ / Raney-Ni / benzene / 5 h / 80 °C / 73550.8 Torr

With hydrogenchloride; sodium tetrahydroborate; sulfur dioxide; hydrogen; nitric acid; sulphurous acid; potassium carbonate; calcium chloride; nickel; In tetrahydrofuran; pyridine; diethyl ether; acetic acid; propionic acid; acetone; benzene;