2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-4-(4-methylphenyl)-1,3-thiazole-5-carboxylic acid

Base Information

Chemical Name:2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-4-(4-methylphenyl)-1,3-thiazole-5-carboxylic acid
CAS No.:1421921-02-9
Molecular Formula:C₂₄H₂₇N₃O₂S
Molecular Weight:421.563
Hs Code.:

Synonyms:2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-4-(4-methylphenyl)-1,3-thiazole-5-carboxylic acid

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Chemical Property of 2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-4-(4-methylphenyl)-1,3-thiazole-5-carboxylic acid

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Technology Process of 2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-4-(4-methylphenyl)-1,3-thiazole-5-carboxylic acid

There total 8 articles about 2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-4-(4-methylphenyl)-1,3-thiazole-5-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methyl 2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-4-(4-methylphenyl)-1,3-thiazole-5-carboxylate dihydrochloride

: 1421921-02-9
2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-4-(4-methylphenyl)-1,3-thiazole-5-carboxylic acid

Guidance literature:: With lithium hydroxide monohydrate; In tetrahydrofuran; water; at 20 ℃; for 4h;

Reference yield:

: 16213-85-7
(2,5-dimethylphenyl)acetonitrile

: 1421921-02-9
2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-4-(4-methylphenyl)-1,3-thiazole-5-carboxylic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: nitric acid / 0.5 h / Cooling with ice

2.1: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

3.1: isopropyl alcohol / 2 h / 80 °C

4.1: ammonium chloride; iron; water / ethanol / 2 h / Reflux

5.1: oxalyl dichloride / chloroform / 0.17 h / 20 °C / Inert atmosphere

5.2: 1 h / 20 °C / Inert atmosphere

6.1: lithium hydroxide monohydrate / water; tetrahydrofuran / 4 h / 20 °C

With hydrogenchloride; oxalyl dichloride; lithium hydroxide monohydrate; water; nitric acid; iron; ammonium chloride; O,O-Diethyl hydrogen phosphorodithioate; In tetrahydrofuran; ethanol; chloroform; water; ethyl acetate; isopropyl alcohol;

Reference yield:

: 1421922-03-3
(2,5-dimethyl-4-nitrophenyl)acetonitrile

: 1421921-02-9
2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-4-(4-methylphenyl)-1,3-thiazole-5-carboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

2.1: isopropyl alcohol / 2 h / 80 °C

3.1: ammonium chloride; iron; water / ethanol / 2 h / Reflux

4.1: oxalyl dichloride / chloroform / 0.17 h / 20 °C / Inert atmosphere

4.2: 1 h / 20 °C / Inert atmosphere

5.1: lithium hydroxide monohydrate / water; tetrahydrofuran / 4 h / 20 °C

With hydrogenchloride; oxalyl dichloride; lithium hydroxide monohydrate; water; iron; ammonium chloride; O,O-Diethyl hydrogen phosphorodithioate; In tetrahydrofuran; ethanol; chloroform; water; ethyl acetate; isopropyl alcohol;