dichlorozinc;N'-[[10-[[2-(dimethylamino)ethyl-methylamino]methyl]anthracen-9-yl]methyl]-N,N,N'-trimethylethane-1,2-diamine

Base Information

• Chemical Name: dichlorozinc;N'-[[10-[[2-(dimethylamino)ethyl-methylamino]methyl]anthracen-9-yl]methyl]-N,N,N'-trimethylethane-1,2-diamine
• CAS No.: 106682-14-8
• Molecular Formula: C₂₆H₃₈Cl₄N₄Zn₂
• Molecular Weight: 679.207
• European Community (EC) Number: 635-164-8
• DSSTox Substance ID: DTXSID60550132
• Mol file: 106682-14-8.mol

Synonyms:106682-14-8;dichlorozinc;N'-[[10-[[2-(dimethylamino)ethyl-methylamino]methyl]anthracen-9-yl]methyl]-N,N,N'-trimethylethane-1,2-diamine;SCHEMBL22261585;DTXSID60550132;N~1~,N~1'~-[Anthracene-9,10-diylbis(methylene)]bis(N~1~,N~2~,N~2~-trimethylethane-1,2-diamine)--dichlorozinc (1/2)

Chemical Property of dichlorozinc;N'-[[10-[[2-(dimethylamino)ethyl-methylamino]methyl]anthracen-9-yl]methyl]-N,N,N'-trimethylethane-1,2-diamine

Chemical Property:

• PSA: 12.96000
• LogP: 6.73280
• Storage Temp.: 2-8°C
• Solubility.: DMSO: soluble
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 10
• Exact Mass: 678.03728
• Heavy Atom Count: 36
• Complexity: 428

Purity/Quality:

99% ^*data from raw suppliers

9,10-Bis(TMEDA)anthracenebiszincchloridecomplex ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)CCN(C)CC1=C2C=CC=CC2=C(C3=CC=CC=C31)CN(C)CCN(C)C.Cl[Zn]Cl.Cl[Zn]Cl
• Uses: 9,10-Bis(TMEDA)anthracene biszinc chloride complex (cas# 106682-14-8) is a compound useful in organic synthesis.

Technology Process of dichlorozinc;N'-[[10-[[2-(dimethylamino)ethyl-methylamino]methyl]anthracen-9-yl]methyl]-N,N,N'-trimethylethane-1,2-diamine

There total 1 articles about dichlorozinc;N'-[[10-[[2-(dimethylamino)ethyl-methylamino]methyl]anthracen-9-yl]methyl]-N,N,N'-trimethylethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

9,10-bis-(((2-(dimethylamino)ethyl)methylamino)methyl)anthracene (106712-13-4) + zinc(II) chloride (7646-85-7,24359-56-6) → (9,10-bis(((2-(dimethylamino)ethyl)methylamino)methyl)anthracene-N,N',N'',N''')dizinc tetrachloride (106682-14-8)

Guidance literature:

In methanol; addn. of ligand soln. to a hot stirred soln. of ZnCl2; cooled slowly to room temp., crystn., filtered, washed (MeOH), dried at 70°C in vac. overnight, elem. anal.;

DOI:10.1021/ja00240a037

upstream raw materials:

9,10-bis-(((2-(dimethylamino)ethyl)methylamino)methyl)anthracene

zinc(II) chloride